4-(ethoxycarbonyl)phenyl 2,4,6-tri-t-butylphenyl selenide

Base Information

• Chemical Name: 4-(ethoxycarbonyl)phenyl 2,4,6-tri-t-butylphenyl selenide
• CAS No.: 123133-03-9
• Molecular Formula: C₂₇H₃₈O₂Se
• Molecular Weight: 473.558
• Mol file: 123133-03-9.mol

Synonyms:

Chemical Property of 4-(ethoxycarbonyl)phenyl 2,4,6-tri-t-butylphenyl selenide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-(ethoxycarbonyl)phenyl 2,4,6-tri-t-butylphenyl selenide

There total 2 articles about 4-(ethoxycarbonyl)phenyl 2,4,6-tri-t-butylphenyl selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(ethoxycarbonyl)benzenediazonium chloride (2028-79-7) → 4-(ethoxycarbonyl)phenyl 2,4,6-tri-t-butylphenyl selenide (123133-03-9)

Guidance literature:

Multi-step reaction with 2 steps

2: 1.) BuLi / 1.) hexane, -60 deg C, 2.) THF

With n-butyllithium;

Reference yield:

1-bromo-2,4,6-tri-tert-butylbenzene (3975-77-7) + (4-Ethoxycarbonyl)phenylselenocyanate (1778-11-6) → 4-(ethoxycarbonyl)phenyl 2,4,6-tri-t-butylphenyl selenide (123133-03-9)

Guidance literature:

With n-butyllithium; Yield given. Multistep reaction; 1.) hexane, -60 deg C, 2.) THF;

Reference yield:

4-(ethoxycarbonyl)phenyl 2,4,6-tri-t-butylphenyl selenide (123133-03-9) → 4-carboxyphenyl 2,4,6-tri-t-butylphenyl selenide (123133-04-0)

Guidance literature:

With potassium hydroxide; In methanol; water; Yield given;

upstream raw materials:

1-bromo-2,4,6-tri-tert-butylbenzene

(4-Ethoxycarbonyl)phenylselenocyanate

4-(ethoxycarbonyl)benzenediazonium chloride

Downstream raw materials:

4-carboxyphenyl 2,4,6-tri-t-butylphenyl selenide

4-<(-)-menthyloxycarbonyl>phenyl 2,4,6-tri-t-butylphenyl selenide

(+)-4-(methoxycarbonyl)phenyl 2,4,6-tri-butylphenyl selenoxide

(-)-4-(methoxycarbonyl)phenyl 2,4,6-tri-t-butylphenyl selenoxide