3-Amino-2,6-dibromoisonicotinic acid

Base Information

Chemical Name:3-Amino-2,6-dibromoisonicotinic acid
CAS No.:52834-10-3
Molecular Formula:C₆H₄Br₂N₂O₂
Molecular Weight:295.918
Hs Code.:
Mol file:52834-10-3.mol

Synonyms:

Suppliers and Price of 3-Amino-2,6-dibromoisonicotinic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
Ethyl 3-amino-2,5-dibromoisonicotinate 97%
1g
$ 623.00

Crysdot
3-Amino-2,6-dibromoisonicotinicacid 95+%
1g
$ 586.00

Chemenu
3-Amino-2,6-dibromoisonicotinicacid 95%
1g
$ 554.00

Atlantic Research Chemicals
Ethyl 3-Amino-2,5-dibromoisonicotinate 95%
Price $/1gm:
$ 250.90

Atlantic Research Chemicals
Ethyl 3-Amino-2,5-dibromoisonicotinate 95%
Price $/250mgs:
$ 123.86

Atlantic Research Chemicals
Ethyl 3-Amino-2,5-dibromoisonicotinate 95%
Price $/50mgs:
$ 50.81

Alichem
3-Amino-2,6-dibromoisonicotinicacid
1g
$ 596.40

Total 7 raw suppliers

Chemical Property of 3-Amino-2,6-dibromoisonicotinic acid

Chemical Property:

Vapor Pressure:1.62E-11mmHg at 25°C
Storage Temp.:2-8°C

Purity/Quality:

99% ^*data from raw suppliers

Ethyl 3-amino-2,5-dibromoisonicotinate 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-Amino-2,6-dibromoisonicotinic acid

There total 5 articles about 3-Amino-2,6-dibromoisonicotinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7579-20-6
3-Aminopyridine-4-carboxylic acid

: 52834-10-3
3-Amino-2,6-dibromoisonicotinsaeure

Guidance literature:: In diethyl ether; bromine; acetic acid;

Reference yield:

: 462-08-8
pyridin-3-ylamine

: 52834-10-3
3-Amino-2,6-dibromoisonicotinsaeure

Guidance literature:: Multi-step reaction with 4 steps

1.1: tert-butyl alcohol / 24 h / 20 - 50 °C

2.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / diethyl ether; hexane / -78 - -10 °C

2.2: 0.5 h / -78 °C

2.3: pH ~ 3 / Acidic aqueous solution

3.1: hydrogenchloride; water / methanol / 2.5 h / Heating / reflux

3.2: 20 °C / pH ~ 14

3.3: pH ~ 3

4.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 4 h / 20 °C

4.3: pH ~ 2

With hydrogenchloride; N-Bromosuccinimide; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; water; In methanol; diethyl ether; hexane; N,N-dimethyl-formamide; tert-butyl alcohol;

Reference yield:

: 56700-70-0
3-(tert-butoxycarbonylamino)pyridine

: 52834-10-3
3-Amino-2,6-dibromoisonicotinsaeure

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / diethyl ether; hexane / -78 - -10 °C

1.2: 0.5 h / -78 °C

1.3: pH ~ 3 / Acidic aqueous solution

2.1: hydrogenchloride; water / methanol / 2.5 h / Heating / reflux

2.2: 20 °C / pH ~ 14

2.3: pH ~ 3

3.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 4 h / 20 °C

3.3: pH ~ 2

With hydrogenchloride; N-Bromosuccinimide; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; water; In methanol; diethyl ether; hexane; N,N-dimethyl-formamide;