4-benzoyl-4-ethoxycarbonylheptanedinitrile

Base Information

Chemical Name:4-benzoyl-4-ethoxycarbonylheptanedinitrile
CAS No.:103924-01-2
Molecular Formula:C₁₇H₁₈N₂O₃
Molecular Weight:298.342
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-benzoyl-4-ethoxycarbonylheptanedinitrile

Chemical Property:

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Technology Process of 4-benzoyl-4-ethoxycarbonylheptanedinitrile

There total 1 articles about 4-benzoyl-4-ethoxycarbonylheptanedinitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 94-02-0
ethyl 3-oxo-3-phenylpropionate

: 107-13-1,25014-41-9
acrylonitrile

: 103924-01-2
4-benzoyl-4-ethoxycarbonylheptanedinitrile

Guidance literature:: With N-benzyl-trimethylammonium hydroxide; tert-butyl alcohol;
DOI:10.1021/jo01164a022

Reference yield: 82.0%

: 103924-01-2
4-benzoyl-4-ethoxycarbonylheptanedinitrile

: 103924-02-3
4-benzoyl-4-ethoxycarbonylheptanedioic acid

Guidance literature:: With hydrogenchloride; for 7.25h; Heating;

Reference yield:

: 103924-01-2
4-benzoyl-4-ethoxycarbonylheptanedinitrile

: 103944-69-0
1-benzoyl-10-methyladamantane-2,4,6-trione

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / conc. hydrochloric acid / 7.25 h / Heating

2: 71 percent / acetic anhydride

3: toluene-p-sulphonic acid / benzene / 16 h / Heating

4: 2) water / 1) benzene, reflux, 20 h; 2) 5 h

With hydrogenchloride; water; acetic anhydride; toluene-4-sulfonic acid; In benzene;