Technology Process of [([N-(2,4,6-Me3C6H2)(3-NH-SC4H2-2-)]2PPh))ZrCl2
There total 1 articles about [([N-(2,4,6-Me3C6H2)(3-NH-SC4H2-2-)]2PPh))ZrCl2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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In
toluene;
under N2 or Ar; to a stirred toluene soln. of Zr-contg. compd. (3.56 mmol) was added Me3SiCl (35.6 mmol) dropwise; stirring for 5 h; the react. mixt. was taken to dryness; the compd. was collected on a frit, washed with pentane, and dried; elem. anal.;
DOI:10.1021/om900612n
- Guidance literature:
-
In
toluene;
under N2 or Ar; to a stirred toluene soln. of Zr-contg. compd. (1.28 mmol) was added Me3SiI (12.8 mmol) dropwise; stirring overnight; the react. mixt. was taken to dryness; the compd. was collected on a frit, washed with pentane, and dried; elem. anal.;
DOI:10.1021/om900612n
