Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-10,13-dimethyl-7-(2-1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-yl-acetoxy)-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

Base Information

• Chemical Name: Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-10,13-dimethyl-7-(2-1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-yl-acetoxy)-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester
• CAS No.: 907205-61-2
• Molecular Formula: C₆₂H₇₉NO₁₁
• Molecular Weight: 1014.31

Synonyms:

Chemical Property of Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-10,13-dimethyl-7-(2-1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-yl-acetoxy)-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Useful:

Technology Process of Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-10,13-dimethyl-7-(2-1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-yl-acetoxy)-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

There total 6 articles about Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-10,13-dimethyl-7-(2-1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-yl-acetoxy)-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl 3α,7α-dihydroxy-5β-cholan-24-oate (111992-94-0) → Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-10,13-dimethyl-7-(2-1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-yl-acetoxy)-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester (907205-61-2)

Guidance literature:

Multi-step reaction with 3 steps

1: dicyclohexylcarbodiimide; 4-dimethylaminopyridine / CH₂Cl₂

2: tetrabutylammonium iodide; calcium hydride / toluene / Heating

3: sodium carbonate / acetonitrile / Heating

With dmap; calcium hydride; tetra-(n-butyl)ammonium iodide; sodium carbonate; dicyclohexyl-carbodiimide; In dichloromethane; toluene; acetonitrile;

DOI:10.1021/ol061082k

Reference yield:

Pyrene-1-carboxylic acid (3R,5R,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-7-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester (907205-58-7) → Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-10,13-dimethyl-7-(2-1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-yl-acetoxy)-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester (907205-61-2)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrabutylammonium iodide; calcium hydride / toluene / Heating

2: sodium carbonate / acetonitrile / Heating

With calcium hydride; tetra-(n-butyl)ammonium iodide; sodium carbonate; In toluene; acetonitrile;

DOI:10.1021/ol061082k

Reference yield:

Pyrene-1-carboxylic acid (19694-02-1) → Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-10,13-dimethyl-7-(2-1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-yl-acetoxy)-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester (907205-61-2)

Guidance literature:

Multi-step reaction with 3 steps

1: dicyclohexylcarbodiimide; 4-dimethylaminopyridine / CH₂Cl₂

2: tetrabutylammonium iodide; calcium hydride / toluene / Heating

3: sodium carbonate / acetonitrile / Heating

With dmap; calcium hydride; tetra-(n-butyl)ammonium iodide; sodium carbonate; dicyclohexyl-carbodiimide; In dichloromethane; toluene; acetonitrile;

DOI:10.1021/ol061082k

upstream raw materials:

Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-7-(2-chloro-acetoxy)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

1-aza-18-crown-6

benzyl 3α,7α-dihydroxy-5β-cholan-24-oate

Pyrene-1-carboxylic acid (3R,5R,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-7-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

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