methyl exo-7b-acetyl-3-benzoyl-1,2,2a,7b-tetrahydro-3H-cyclobutindole-1-carboxylate

Base Information

• Chemical Name: methyl exo-7b-acetyl-3-benzoyl-1,2,2a,7b-tetrahydro-3H-cyclobutindole-1-carboxylate
• CAS No.: 90540-01-5
• Molecular Formula: C₂₁H₁₉NO₄
• Molecular Weight: 349.386

Synonyms:

Chemical Property of methyl exo-7b-acetyl-3-benzoyl-1,2,2a,7b-tetrahydro-3H-cyclobutindole-1-carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl exo-7b-acetyl-3-benzoyl-1,2,2a,7b-tetrahydro-3H-cyclobutindole-1-carboxylate

There total 3 articles about methyl exo-7b-acetyl-3-benzoyl-1,2,2a,7b-tetrahydro-3H-cyclobutindole-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-acetylindole (703-80-0) → methyl exo-7b-acetyl-3-benzoyl-1,2,2a,7b-tetrahydro-3H-cyclobutindole-1-carboxylate (90540-01-5,90582-41-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / K₂CO₃ / 1,2-dimethoxy-ethane; H₂O / 6 h / Ambient temperature

2: benzene / 8 h / Irradiation

With potassium carbonate; In 1,2-dimethoxyethane; water; benzene;

DOI:10.1039/P19840000405

Reference yield:

benzoyl chloride (98-88-4) → methyl exo-7b-acetyl-3-benzoyl-1,2,2a,7b-tetrahydro-3H-cyclobutindole-1-carboxylate (90540-01-5,90582-41-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / K₂CO₃ / 1,2-dimethoxy-ethane; H₂O / 6 h / Ambient temperature

2: benzene / 8 h / Irradiation

With potassium carbonate; In 1,2-dimethoxyethane; water; benzene;

DOI:10.1039/P19840000405

Reference yield:

1-(1-benzoyl-1H-indol-3-yl)ethanone (90539-81-4) + acrylic acid methyl ester (292638-85-8,9003-21-8,96-33-3) → methyl 7b-acetyl-3-benzoyl-1,2,2a,7b-tetrahydro-3H-cyclobutindole-2-carboxylate (90540-02-6) + methyl exo-7b-acetyl-3-benzoyl-1,2,2a,7b-tetrahydro-3H-cyclobutindole-1-carboxylate (90540-01-5,90582-41-5) + methyl endo-7b-acetyl-3-benzoyl-1,2,2a,7b-tetrahydro-3H-cyclobutindole-1-carboxylate

Guidance literature:

In benzene; for 8h; Yield given. Yields of byproduct given; Irradiation;

DOI:10.1039/P19840000405

upstream raw materials:

1-(1-benzoyl-1H-indol-3-yl)ethanone

acrylic acid methyl ester

3-acetylindole

benzoyl chloride

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 90540-01-5 methyl exo-7b-acetyl-3-benzoyl-1,2,2a,7b-tetrahydro-3H-cyclobutindole-1-carboxylate

Send

Send

Metric Ton KG G Pound L ML

Send

Send