Dithiophosphoric acid O-[(2R,3R,4R,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-(2-methylsulfanyl-phenylsulfanylmethoxy)-tetrahydro-furan-3-yl] ester S,S'-diphenyl ester

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Chemical Name:Dithiophosphoric acid O-[(2R,3R,4R,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-(2-methylsulfanyl-phenylsulfanylmethoxy)-tetrahydro-furan-3-yl] ester S,S'-diphenyl ester
CAS No.:132609-74-6
Molecular Formula:C₅₇H₅₂N₃O₉PS₄
Molecular Weight:1082.29
Hs Code.:

Dithiophosphoric acid O-[(2R,3R,4R,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-(2-methylsulfanyl-phenylsulfanylmethoxy)-tetrahydro-furan-3-yl] ester S,S'-diphenyl ester

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Chemical Property of Dithiophosphoric acid O-[(2R,3R,4R,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-(2-methylsulfanyl-phenylsulfanylmethoxy)-tetrahydro-furan-3-yl] ester S,S'-diphenyl ester

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Technology Process of Dithiophosphoric acid O-[(2R,3R,4R,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-(2-methylsulfanyl-phenylsulfanylmethoxy)-tetrahydro-furan-3-yl] ester S,S'-diphenyl ester

There total 5 articles about Dithiophosphoric acid O-[(2R,3R,4R,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-(2-methylsulfanyl-phenylsulfanylmethoxy)-tetrahydro-furan-3-yl] ester S,S'-diphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 86365-02-8
2'-O-(1,3-benzodithiol-2-yl)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine

: 132609-74-6
Dithiophosphoric acid O-[(2R,3R,4R,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-(2-methylsulfanyl-phenylsulfanylmethoxy)-tetrahydro-furan-3-yl] ester S,S'-diphenyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: tributyltin hydride, azobisisobutyronitrile / benzene / 2 h / Heating

2: dimethylformamide / 2 h

3: 79 percent / phosphoryl chloride

4: 87 percent

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; trichlorophosphate; In N,N-dimethyl-formamide; benzene;

Reference yield:

: 1-[(2R,3R,3aR,9aR)-5,5,7,7-Tetraisopropyl-3-(2-mercapto-phenylsulfanylmethoxy)-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl]-1H-pyrimidine-2,4-dione

: 132609-74-6
Dithiophosphoric acid O-[(2R,3R,4R,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-(2-methylsulfanyl-phenylsulfanylmethoxy)-tetrahydro-furan-3-yl] ester S,S'-diphenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: dimethylformamide / 2 h

2: 79 percent / phosphoryl chloride

3: 87 percent

With trichlorophosphate; In N,N-dimethyl-formamide;