2'-O-(1,3-benzodithiol-2-yl)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxan-1,3-diyl)uridine

Base Information

Chemical Name:2'-O-(1,3-benzodithiol-2-yl)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxan-1,3-diyl)uridine
CAS No.:86365-02-8
Molecular Formula:C28H42N2O7S2Si2
Molecular Weight:638.954
Hs Code.:
Mol file:86365-02-8.mol

Synonyms:2'-O-(1,3-benzodithiol-2-yl)-3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)uridine;

Suppliers and Price of 2'-O-(1,3-benzodithiol-2-yl)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxan-1,3-diyl)uridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2'-O-(1,3-benzodithiol-2-yl)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxan-1,3-diyl)uridine

Chemical Property:

PSA：151.61000
Density:1.25g/cm³
LogP:5.95720

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2'-O-(1,3-benzodithiol-2-yl)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxan-1,3-diyl)uridine

There total 1 articles about 2'-O-(1,3-benzodithiol-2-yl)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxan-1,3-diyl)uridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57842-27-0
1,3-benzodithiol-2-ylium tetrafluoroborate

: 69304-38-7
3',5'-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine

: 86365-02-8
2'-O-(1,3-benzodithiol-2-yl)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine

Guidance literature:: With pyridine; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1021/jo00166a039

Reference yield:

: 86365-02-8
2'-O-(1,3-benzodithiol-2-yl)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine

: 2140-76-3
2'-O-methyluridine

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / Raney Ni / ethanol / 1.5 h / Heating

2: 78 percent / KF-Et₄NBr / methanol; H₂O

With potassium fluoride; tetraethylammonium bromide; nickel; In methanol; ethanol; water;
DOI:10.1021/jo00231a052

Reference yield:

: 86365-02-8
2'-O-(1,3-benzodithiol-2-yl)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine

: 1-{(2R,3R,4R,5R)-3-(Benzo[1,3]dithiol-2-yloxy)-5-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-hydroxy-tetrahydro-furan-2-yl}-1H-pyrimidine-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / potassium fluoride, tetraethylammonium bromide / acetonitrile; H₂O / 1 h / 60 °C

2: pyridine / 9 h / Ambient temperature

With potassium fluoride; tetraethylammonium bromide; In pyridine; water; acetonitrile;
DOI:10.1021/jo00166a039