C₂₅H₃₂N₂O₇S

Base Information

Chemical Name:C₂₅H₃₂N₂O₇S
CAS No.:476182-10-2
Molecular Formula:C₂₅H₃₂N₂O₇S
Molecular Weight:504.604
Hs Code.:

C<sub>25</sub>H<sub>32</sub>N<sub>2</sub>O<sub>7</sub>S

Synonyms:

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Chemical Property of C₂₅H₃₂N₂O₇S

Chemical Property:

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Technology Process of C₂₅H₃₂N₂O₇S

There total 10 articles about C₂₅H₃₂N₂O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 476192-12-8
4-[(4-fluorophenyl)sulfonyl]tetrahydro-2H-pyran-4-carboxylic acid, 1,1-dimethylethyl ester

: 476182-10-2
C₂₅H₃₂N₂O₇S

Guidance literature:: Multi-step reaction with 8 steps

1: sodium hydride / 4 h / 0 - 20 °C

2: 5% Pd(II)/C(eggshell) / tetrahydrofuran / 1.5 h / 4137.29 Torr

3: sodium periodate; ruthenium trichloride / tetrachloromethane; water

4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 16 h

5: trifluoroacetic acid

6: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 19.5 h / 20 - 40 °C

7: tetrahydrofuran / 0 - 20 °C

8: hydrogenchloride; water / 1,4-dioxane; methanol

With hydrogenchloride; ruthenium trichloride; sodium periodate; 5% Pd(II)/C(eggshell); water; sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; methanol; tetrachloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.03.095

Reference yield:

: 476192-21-9
C₂₃H₃₅NO₈S

: 476182-10-2
C₂₅H₃₂N₂O₇S

Guidance literature:: Multi-step reaction with 4 steps

1: trifluoroacetic acid

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 19.5 h / 20 - 40 °C

3: tetrahydrofuran / 0 - 20 °C

4: hydrogenchloride; water / 1,4-dioxane; methanol

With hydrogenchloride; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.03.095

Reference yield:

: 476194-63-5
tetrahydro-4-[[4-[[5-(methoxy-methylamino)-5-oxopentyl]oxy]phenyl]sulfonyl]-N-[(tetrahydro-2H-pyran-2-yl)oxy]-2H-pyran-4-carboxamide

: 476182-10-2
C₂₅H₃₂N₂O₇S

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 0 - 20 °C

2: hydrogenchloride; water / 1,4-dioxane; methanol

With hydrogenchloride; water; In tetrahydrofuran; 1,4-dioxane; methanol;
DOI:10.1016/j.bmcl.2011.03.095