[Ru(C₅H₅)(P(C₆H₅)3)(C₅H₄N(CH₃))(CN)]

Base Information

Chemical Name:[Ru(C₅H₅)(P(C₆H₅)3)(C₅H₄N(CH₃))(CN)]
CAS No.:97286-32-3
Molecular Formula:C₃₀H₂₇N₂PRu
Molecular Weight:547.602
Hs Code.:

[Ru(C<sub>5</sub>H<sub>5</sub>)(P(C<sub>6</sub>H<sub>5</sub>)3)(C<sub>5</sub>H<sub>4</sub>N(CH<sub>3</sub>))(CN)]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Ru(C₅H₅)(P(C₆H₅)3)(C₅H₄N(CH₃))(CN)]

Chemical Property:

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Technology Process of [Ru(C₅H₅)(P(C₆H₅)3)(C₅H₄N(CH₃))(CN)]

There total 1 articles about [Ru(C₅H₅)(P(C₆H₅)3)(C₅H₄N(CH₃))(CN)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-99-6
3-Methylpyridine

: 55272-32-7
[Ru(η5-Cp)(triphenylphosphine)2(CN)]

: 97286-32-3
[Ru(C₅H₅)(P(C₆H₅)3)(C₅H₄N(CH₃))(CN)]

Guidance literature:: In further solvent(s); (Ru(η-C5H5)(PPh3)2(CN)) heated under reflux for 10 h in 3-picoline under N2 atm.; crystals centrifuged, washed with ethanol, water, ethanol and diethyl ether and dried in vacuo and recrystd. from CH2Cl2/light petroleum (40-60°C); elem. anal.;
DOI:10.1016/S0020-1693(00)87599-4

Reference yield:

: 13444-89-8
nitrosyl tribromide

: 97286-32-3
[Ru(C₅H₅)(P(C₆H₅)3)(C₅H₄N(CH₃))(CN)]

: 97263-26-8
[Ru(NO)(P(C₆H₅)3)(C₅H₄N(CH₃))Br₃]

Guidance literature:: With triphenylphosphine; In methanol; dichloromethane; under pure and dry nitrogen; slow addn. of a satd. soln. of the NO-compd. in CH2Cl2 to a soln. of the Ru-compd. in CH2Cl2/MeOH, while heating under reflux for 30 min addn. of triphenylphosphine; crystals are sepd., washed with MeOH and ether and finally dried in vac.; elem. anal.;

Reference yield:

: 97286-32-3
[Ru(C₅H₅)(P(C₆H₅)3)(C₅H₄N(CH₃))(CN)]

: 2696-92-6
nitrosylchloride

: (Ru(NO)(P(C₆H₅)3)(NC₅H₄CH₃)Cl₃)

Guidance literature:: In methanol; dichloromethane; to soln. (Ru(η5-C5H5)(PPh3)(3-Pic)(CN)) in CH2Cl2 methanol added, followed by addn. saturated CH2Cl2 soln. NOCl, react. mixt. heated under reflux for 30 min under N2 atm.; elem. anal.;
DOI:10.1016/S0020-1693(00)87600-8