1,4-(p-PhCB₁₀H₁₀C)2C₆F₄

Base Information

Chemical Name:1,4-(p-PhCB₁₀H₁₀C)2C₆F₄
CAS No.:265987-31-3
Molecular Formula:C₂₂H₃₀B₂₀F₄
Molecular Weight:586.694
Hs Code.:

1,4-(p-PhCB<sub>10</sub>H<sub>10</sub>C)2C<sub>6</sub>F<sub>4</sub>

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Chemical Property of 1,4-(p-PhCB₁₀H₁₀C)2C₆F₄

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Technology Process of 1,4-(p-PhCB₁₀H₁₀C)2C₆F₄

There total 1 articles about 1,4-(p-PhCB₁₀H₁₀C)2C₆F₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 392-56-3
Hexafluorobenzene

: 53065-73-9
1-phenyl-1,12-dicarba-closo-dodecaborane

: 265987-30-2
1,12-PhCB₁₀H₁₀CC₆F₅

: 265987-31-3
1,4-(p-PhCB₁₀H₁₀C)2C₆F₄

Guidance literature:: With n-C₄H₉Li; In diethyl ether; hexane; 1-Ph-p-carborane in dry Et2O added slowly with n-C4H9Li in hexane at 0°C under N2, warmed to room temp. with stirring, added dropwise toC6F6 (excess) in Et2O at 0°C, stirred for 24 h at room temp.; washed with dild. acid, filtered, insol. solid filtered off, ether layer washed, dried, solvent removed, combined with the insol. solid, extd. (hot MeCN), crystd. on cooling; elem. anal.;
DOI:10.1016/S0022-328X(99)00672-5