N-[1-(2,3-dihydro-1-benzofuran-5-yl)ethylidene]hydroxylamine

Base Information

Chemical Name:N-[1-(2,3-dihydro-1-benzofuran-5-yl)ethylidene]hydroxylamine
CAS No.:146321-88-2
Molecular Formula:C₁₀H₁₁NO₂
Molecular Weight:177.203
Hs Code.:
DSSTox Substance ID:DTXSID90430559

Synonyms:146321-88-2;N-[1-(2,3-dihydro-1-benzofuran-5-yl)ethylidene]hydroxylamine;5-Acetyl-2,3-dihydrobenzofuran oxime;(NE)-N-[1-(2,3-dihydro-1-benzofuran-5-yl)ethylidene]hydroxylamine;SCHEMBL2244076;DTXSID90430559;HMS1527H18;5-Acetyl-2,3-dihydrobenzofuranoxime;AKOS026672008;FS-5553;NCGC00176720-01;EN300-59892;A921487;BRD-K16242100-001-01-2;Z232287670;N-[(1E)-1-(2,3-Dihydro-1-benzofuran-5-yl)ethylidene]hydroxylamine

Suppliers and Price of N-[1-(2,3-dihydro-1-benzofuran-5-yl)ethylidene]hydroxylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
N-[1-(2,3-Dihydro-1-benzofuran-5-yl)ethylidene]hydroxylamine
50mg
$ 45.00

Crysdot
5-Acetyl-2,3-dihydrobenzofuranoxime 95+%
5g
$ 307.00

AK Scientific
N-[1-(2,3-Dihydro-1-benzofuran-5-yl)ethylidene]hydroxylamine
2.5g
$ 279.00

AK Scientific
N-[1-(2,3-Dihydro-1-benzofuran-5-yl)ethylidene]hydroxylamine
100mg
$ 170.00

Total 2 raw suppliers

Chemical Property of N-[1-(2,3-dihydro-1-benzofuran-5-yl)ethylidene]hydroxylamine

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:177.078978594
Heavy Atom Count:13
Complexity:215

Purity/Quality:

97% ^*data from raw suppliers

N-[1-(2,3-Dihydro-1-benzofuran-5-yl)ethylidene]hydroxylamine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=NO)C1=CC2=C(C=C1)OCC2
Isomeric SMILES:C/C(=N\O)/C1=CC2=C(C=C1)OCC2

Technology Process of N-[1-(2,3-dihydro-1-benzofuran-5-yl)ethylidene]hydroxylamine

There total 3 articles about N-[1-(2,3-dihydro-1-benzofuran-5-yl)ethylidene]hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 90843-31-5
1-(2,3-dihydrobenzofuran-5-yl)ethanone

: 146321-88-2
1-(2,3-dihydro-1-benzofuran-5-yl)ethanone oxime

Guidance literature:: With hydroxylamine hydrochloride; triethylamine; In ethanol; for 25h;
DOI:10.1016/j.bmcl.2004.06.035

Reference yield:

: 252978-89-5
4-(1H-indol-4-yl)-piperazine-1-carboxylic acid tert-butyl ester

: 90843-31-5
1-(2,3-dihydrobenzofuran-5-yl)ethanone

: 146321-88-2
1-(2,3-dihydro-1-benzofuran-5-yl)ethanone oxime

Guidance literature:: 1-(2,3-dihydrobenzofuran-5-yl)ethanone; With hydroxylamine hydrochloride; In methanol; at 20 ℃;

4-(1H-indol-4-yl)-piperazine-1-carboxylic acid tert-butyl ester;

Reference yield:

: 496-16-2
2.3-dihydrobenzofuran

: 146321-88-2
1-(2,3-dihydro-1-benzofuran-5-yl)ethanone oxime

Guidance literature:: Multi-step reaction with 2 steps

1.1: aluminum (III) chloride / dichloromethane / 0.25 h / -10 °C

1.2: 0.5 h / -10 °C

1.3: 2 h / 0 °C

2.1: pyridine; hydroxylamine hydrochloride / methanol / 16 h / 20 °C

With pyridine; aluminum (III) chloride; hydroxylamine hydrochloride; In methanol; dichloromethane;