chlorodiphenyltin(IV) 9-(butylaminomethyl)-anthracenyl dithiocarbamate

Base Information

• Chemical Name: chlorodiphenyltin(IV) 9-(butylaminomethyl)-anthracenyl dithiocarbamate
• CAS No.: 1204529-76-9
• Molecular Formula: C₃₂H₃₀ClNS₂Sn
• Molecular Weight: 646.892
• Mol file: 1204529-76-9.mol

Synonyms:

Chemical Property of chlorodiphenyltin(IV) 9-(butylaminomethyl)-anthracenyl dithiocarbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of chlorodiphenyltin(IV) 9-(butylaminomethyl)-anthracenyl dithiocarbamate

There total 1 articles about chlorodiphenyltin(IV) 9-(butylaminomethyl)-anthracenyl dithiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.4%

carbon disulfide (75-15-0,12122-00-8) + diphenyltin(IV) dichloride (1135-99-5) + N-butylamine (109-73-9,85404-21-3) + 9-anthracene aldehyde (642-31-9) → chlorodiphenyltin(IV) 9-(butylaminomethyl)-anthracenyl dithiocarbamate (1204529-76-9)

Guidance literature:

With NaBH₄; NaOH; In sodium hydroxide; ethanol; aq. NaOH; to soln. of 9-CHO-anthracene in EtOH BuNH2d added, reflux (4 h), treated(NaBH4, stirring, 0°C), stirring at room temp. (8 h), washing (H 2O); org. phase dissolved in EtOH, treated (NaOH, CS2), stirred (18 h, room temp.), Ph2Cl2Sn added, 2 h; filtration; elem. anal.;

DOI:10.1016/j.poly.2009.09.010

upstream raw materials:

carbon disulfide

diphenyltin(IV) dichloride

N-butylamine

9-anthracene aldehyde