Ph₂Sn[1-(4-hydroxyphenyl)-1H-tetrazole-5-thiol^(1-)]2

Base Information

Chemical Name:Ph₂Sn[1-(4-hydroxyphenyl)-1H-tetrazole-5-thiol^(1-)]2
CAS No.:726181-15-3
Molecular Formula:C₂₆H₂₀N₈O₂S₂Sn
Molecular Weight:659.339
Hs Code.:

Ph<sub>2</sub>Sn[1-(4-hydroxyphenyl)-1H-tetrazole-5-thiol<sup>(1-)</sup>]2

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Chemical Property of Ph₂Sn[1-(4-hydroxyphenyl)-1H-tetrazole-5-thiol^(1-)]2

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Technology Process of Ph₂Sn[1-(4-hydroxyphenyl)-1H-tetrazole-5-thiol^(1-)]2

There total 1 articles about Ph₂Sn[1-(4-hydroxyphenyl)-1H-tetrazole-5-thiol^(1-)]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1135-99-5
diphenyltin(IV) dichloride

: 52431-78-4
1-(4-hydroxyphenyl)-1H-tetrazole-5-thiol

: 726181-15-3
Ph₂Sn[1-(4-hydroxyphenyl)-1H-tetrazole-5-thiol^(1-)]2

Guidance literature:: With sodium ethoxide; In ethanol; reaction carried out under N2, organic thiol added to a soln. of NaOEt in ethanol, stirred for 10 min, Ph2SnCl2 added, reaction continued for 12h at 50 °C, cooled down to room temp., filtered; solvent gradually removed by evapn. under vacuum, recrystallized from ether-petroleum, elem. anal.;
DOI:10.1016/j.poly.2004.03.003