[Ru(η6-p-cymene)(2,2,6,6-tetraazaheptane-3,5-dione(-H))(1,3,5-triaza-7-phosphaadamantane)][BPh4]

Base Information

Chemical Name:[Ru(η6-p-cymene)(2,2,6,6-tetraazaheptane-3,5-dione(-H))(1,3,5-triaza-7-phosphaadamantane)][BPh4]
CAS No.:1104968-39-9
Molecular Formula:C₂₄H₂₀B*C₂₇H₄₅N₃O₂PRu
Molecular Weight:894.951
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Ru(η6-p-cymene)(2,2,6,6-tetraazaheptane-3,5-dione(-H))(1,3,5-triaza-7-phosphaadamantane)][BPh4]

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Technology Process of [Ru(η6-p-cymene)(2,2,6,6-tetraazaheptane-3,5-dione(-H))(1,3,5-triaza-7-phosphaadamantane)][BPh4]

There total 1 articles about [Ru(η6-p-cymene)(2,2,6,6-tetraazaheptane-3,5-dione(-H))(1,3,5-triaza-7-phosphaadamantane)][BPh4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: [Ru(η6-p-cymene)(tBu2acac)Cl]

: 143-66-8
sodium tetraphenyl borate

: 53597-69-6
(1,3,5-triaza-7-phosphaadamantane)

: 1104968-39-9
[Ru(η6-p-cymene)(2,2,6,6-tetraazaheptane-3,5-dione(-H))(1,3,5-triaza-7-phosphaadamantane)][BPh4]

Guidance literature:: In dichloromethane; acetone; NaBPh4 (0.231 mmol) and PTA (0.229 mmol) added to soln. of Ru compd. (0.220 mmol) in acetone and CH2Cl2 at room temp., mixt. refluxed, stirred at room temp. for 15 min, heating/stirring cycles repeated for 3 times; evapd., extd. (CH2Cl2), filtered, concd., pptd. (Et2O/petroleum ether), filtered off, washed (petroleum ether), dried (vac.), recrystd. (CHCl3/Et2O, 4°C, 36 h), elem. anal.;
DOI:10.1002/ejic.200701291