dichloro[1,4-bis((diphenylphosphino)ethylmethylene)cyclohexane]platinum

Base Information

Chemical Name:dichloro[1,4-bis((diphenylphosphino)ethylmethylene)cyclohexane]platinum
CAS No.:1000811-24-4
Molecular Formula:C₃₆H₃₈Cl₂P₂Pt
Molecular Weight:798.631
Hs Code.:

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Chemical Property of dichloro[1,4-bis((diphenylphosphino)ethylmethylene)cyclohexane]platinum

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Technology Process of dichloro[1,4-bis((diphenylphosphino)ethylmethylene)cyclohexane]platinum

There total 3 articles about dichloro[1,4-bis((diphenylphosphino)ethylmethylene)cyclohexane]platinum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 12080-32-9
dichloro( 1,5-cyclooctadiene)platinum(ll)

: 1,2-bis(1-(diphenylphosphino)prop-1-ylidene)cyclohexane

: 1000811-24-4,675825-04-4
dichloro[1,4-bis((diphenylphosphino)ethylmethylene)cyclohexane]platinum

Guidance literature:: In dichloromethane; under inert atm. soln. ((COD)PtCl2) in CH2Cl2 was added to soln. diphosphine in CH2Cl2 and stirred for 4 h; react. mixt. was filtered, solvent was removed, residue was crystd. by slow diffusion hexane in CHCl3 soln. at room temp.; elem. anal.;
DOI:10.1021/om034289f

Reference yield: 71.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 827336-49-2,622853-44-5
δ-[(1,2-bis((diphenylphosphino)ethylmethylene)cyclohexane)Pt((S)-BINOL)]

: 1000811-24-4,675825-04-4
δ-[(1,2-bis((diphenylphosphino)ethylmethylene)cyclohexane)PtCl2]

Guidance literature:: In diethyl ether; dichloromethane; byproducts: BINOL; a soln. of Pt complex in CH2Cl2 treated with a soln. of HCl in Et2O; filtered, evapd. (vac.), washed (Et2O, hexane), crystd. by diffusion of a CHCl3 soln. layered with hexane at -20°C; elem. anal.;
DOI:10.1021/om0505716