2-diphenylphosphinobenzoic acid anhydride

Base Information

Chemical Name:2-diphenylphosphinobenzoic acid anhydride
CAS No.:954142-58-6
Molecular Formula:C₃₈H₂₈O₃P₂
Molecular Weight:594.586
Hs Code.:

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Chemical Property of 2-diphenylphosphinobenzoic acid anhydride

Chemical Property:

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Technology Process of 2-diphenylphosphinobenzoic acid anhydride

There total 1 articles about 2-diphenylphosphinobenzoic acid anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 17261-28-8
ortho-diphenylphosphinobenzoic acid

: 954142-58-6
2-diphenylphosphinobenzoic acid anhydride

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; for 3h;
DOI:10.1021/om200073k

Reference yield: 30.0%

: 75-09-2
dichloromethane

: (benzylideneacetone)Fe(CO)3

: 954142-58-6
2-diphenylphosphinobenzoic acid anhydride

: (2-diphenylphosphinobenzoyl)(2-diphenylphosphinobenzoato)iron(II)dicarbonyl*(dichloromethane)

Guidance literature:: In tetrahydrofuran; under Ar; soln. of Fe complex in THF added to slurry of ligand in THF; stirred at reflux for 1 h; solvent removed at reduced pressure; oil triturated with pentane; powderdissolved in CH2Cl2; layered with pentane; crystd. at -35°C for 12 h; filtered; dried under N2 stream; elem. anal.;
DOI:10.1021/om200073k

Reference yield:

: 15321-51-4
diiron nonacarbonyl

: 75-09-2
dichloromethane

: 954142-58-6
2-diphenylphosphinobenzoic acid anhydride

: (2-diphenylphosphinobenzoyl)(2-diphenylphosphinobenzoato)iron(II)dicarbonyl*(dichloromethane)

Guidance literature:: In tetrahydrofuran; under Ar; soln. of Fe complex in THF added to slurry of ligand in THF; stirred at reflux for 1 h; solvent removed at reduced pressure; oil triturated with pentane; powderdissolved in CH2Cl2; layered with pentane; crystd. at -35°C for 12 h; filtered; dried under N2 stream; elem. anal.;
DOI:10.1021/om200073k