N-benzyloxycarbonyl-alanyl--seryl-alanine tert-butyl ester

Base Information

Chemical Name:N-benzyloxycarbonyl-alanyl--seryl-alanine tert-butyl ester
CAS No.:144923-66-0
Molecular Formula:C₂₉H₄₄N₄O₁₂
Molecular Weight:640.688
Hs Code.:

N-benzyloxycarbonyl-alanyl-<O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)>-seryl-alanine tert-butyl ester

Synonyms:

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Chemical Property of N-benzyloxycarbonyl-alanyl--seryl-alanine tert-butyl ester

Chemical Property:

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Technology Process of N-benzyloxycarbonyl-alanyl--seryl-alanine tert-butyl ester

There total 9 articles about N-benzyloxycarbonyl-alanyl--seryl-alanine tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104655-87-0
3,4,6-tri-O-acetyl-2-N-allyloxycarbonyl-2-amino-2-deoxy-α-D-glucopyranosyl bromide

: 144923-66-0
N-benzyloxycarbonyl-alanyl--seryl-alanine tert-butyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 54 percent / molecular sieves 4A, mercuric cyanide / CH₂Cl₂ / 4 h / Ambient temperature

2: dimethyl malonate, tetrakis(triphenylphosphine)palladium⁽⁰⁾ / tetrahydrofuran / 24 h

3: pyridine / 1 h / Ambient temperature

4: 98 percent / H₂ / 10percent Pd/C / methanol / 6 h

5: 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide (EDAC) / CH₂Cl₂ / 72 h

6: hydrazine / methanol / 1 h / Ambient temperature

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 4 A molecular sieve; hydrogen; mercury(II) cyanide; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; malonic acid dimethyl ester; hydrazine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/S0957-4166(00)80230-X

Reference yield:

: N-benzyloxycarbonyl-O-(3,4,6-tri-O-acetyl-2-deoxy-2-acetamido-β-D-glucopyranosyl)-seryl-alanine tert-butyl ester

: 144923-66-0
N-benzyloxycarbonyl-alanyl--seryl-alanine tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / H₂ / 10percent Pd/C / methanol / 6 h

2: 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide (EDAC) / CH₂Cl₂ / 72 h

3: hydrazine / methanol / 1 h / Ambient temperature

With hydrogen; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; hydrazine; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1016/S0957-4166(00)80230-X

Reference yield:

: 24864-42-4
N-benzyloxycarbonyl-seryl-alanine tert-butyl ester

: 144923-66-0
N-benzyloxycarbonyl-alanyl--seryl-alanine tert-butyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 54 percent / molecular sieves 4A, mercuric cyanide / CH₂Cl₂ / 4 h / Ambient temperature

2: dimethyl malonate, tetrakis(triphenylphosphine)palladium⁽⁰⁾ / tetrahydrofuran / 24 h

3: pyridine / 1 h / Ambient temperature

4: 98 percent / H₂ / 10percent Pd/C / methanol / 6 h

5: 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide (EDAC) / CH₂Cl₂ / 72 h

6: hydrazine / methanol / 1 h / Ambient temperature

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 4 A molecular sieve; hydrogen; mercury(II) cyanide; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; malonic acid dimethyl ester; hydrazine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/S0957-4166(00)80230-X