[(OC(CF₃)2CH₂P(C₆H₅)2)2Pd]

Base Information

Chemical Name:[(OC(CF₃)2CH₂P(C₆H₅)2)2Pd]
CAS No.:105119-02-6
Molecular Formula:C₃₂H₂₄F₁₂O₂P₂Pd
Molecular Weight:836.89
Hs Code.:

[(OC(CF<sub>3</sub>)2CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2Pd]

Synonyms:

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Chemical Property of [(OC(CF₃)2CH₂P(C₆H₅)2)2Pd]

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Technology Process of [(OC(CF₃)2CH₂P(C₆H₅)2)2Pd]

There total 1 articles about [(OC(CF₃)2CH₂P(C₆H₅)2)2Pd] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15617-18-2,39958-10-6,14220-64-5
bis(benzonitrile)palladium(II) dichloride

: 98331-76-1
2-[(diphenylphosphanyl)methyl]-1,1,1,3,3,3-hexafluoro-propan-2-ol

: 105119-02-6,98331-70-5
[(OC(CF₃)2CH₂P(C₆H₅)2)2Pd]

Guidance literature:: With KOH; In chloroform; byproducts: KCl; dissolving PdCl2(C6H5CN)2 in CHCl3; addn. of ethanolic soln. of ligand;dropwise addn. of ethanolic KOH soln.;; centrifugation; stirring for 24 h at 25°C; centrifugation; vac. evapn.; addn. of CHCl3; pptn.; elem. anal.;;

Reference yield: 91.0%

: 15617-18-2,39958-10-6,14220-64-5
bis(benzonitrile)palladium(II) dichloride

: 105119-02-6,98331-70-5
[(OC(CF₃)2CH₂P(C₆H₅)2)2Pd]

: 105059-05-0
[(OC(CF₃)2CH₂P(C₆H₅)2PdCl)2]

Guidance literature:: In chloroform; acetone; dissolving Pd(P(C6H5)2CH2C(CF3)2O)2 in CHCl3 containing 10% acetone (50ml); heating to reflux; dropwise addn. of PdCl2((C6H5)CN)2 (0.46g) in CHCl3 (25ml); refluxing, 1h;; concg. soln. to about 20ml volume by rotary evapn.; addn. to 40/60 petroleum ether (about 200ml), formation of ppt.; removal of ppt. by filtration, washing with petroleum ether;;
DOI:10.1016/S0020-1693(00)82183-0

Reference yield:

: 105119-02-6,98331-70-5
[(OC(CF₃)2CH₂P(C₆H₅)2)2Pd]

: 105059-08-3
[OC(CF₃)2CH₂P(C₆H₅)2PdCl(P(CH₃)3)]

Guidance literature:: Multi-step reaction with 2 steps

1: acetone; chloroform

2: ethanol

In ethanol; chloroform; acetone;
DOI:10.1016/S0020-1693(00)82183-0