C₂₃H₂₁F₃N₂O₃S₂

Base Information

Chemical Name:C₂₃H₂₁F₃N₂O₃S₂
CAS No.:1616969-88-0
Molecular Formula:C₂₃H₂₁F₃N₂O₃S₂
Molecular Weight:494.559
Hs Code.:

C<sub>23</sub>H<sub>21</sub>F<sub>3</sub>N<sub>2</sub>O<sub>3</sub>S<sub>2</sub>

Synonyms:

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Chemical Property of C₂₃H₂₁F₃N₂O₃S₂

Chemical Property:

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Technology Process of C₂₃H₂₁F₃N₂O₃S₂

There total 5 articles about C₂₃H₂₁F₃N₂O₃S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 455-19-6
4-Trifluoromethylbenzaldehyde

: 1616969-88-0
C₂₃H₂₁F₃N₂O₃S₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: acetic acid; sodium acetate / 1 h / 80 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / Inert atmosphere

2.2: 1.83 h / Inert atmosphere; Reflux

3.1: n-butyllithium; N-ethyl-N,N-diisopropylamine / tetrahydrofuran; hexane / 0.5 h / -74 °C / Inert atmosphere

3.2: 1 h / Inert atmosphere

4.1: chiralpak IA / hexane; dichloromethane; isopropyl alcohol / Resolution of racemate

5.1: trifluoroacetic acid / 1 h / Reflux

With n-butyllithium; sodium acetate; sodium hydride; acetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; hexane; dichloromethane; isopropyl alcohol; mineral oil;
DOI:10.1002/cmdc.201300553

Reference yield:

: (Z)-5-(4-α,α,α-trifluoromethylbenzylidene)-2-thioxothiazolidin-4-one

: 1616969-88-0
C₂₃H₂₁F₃N₂O₃S₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / Inert atmosphere

1.2: 1.83 h / Inert atmosphere; Reflux

2.1: n-butyllithium; N-ethyl-N,N-diisopropylamine / tetrahydrofuran; hexane / 0.5 h / -74 °C / Inert atmosphere

2.2: 1 h / Inert atmosphere

3.1: chiralpak IA / hexane; dichloromethane; isopropyl alcohol / Resolution of racemate

4.1: trifluoroacetic acid / 1 h / Reflux

With n-butyllithium; sodium hydride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; hexane; dichloromethane; isopropyl alcohol; mineral oil;
DOI:10.1002/cmdc.201300553

Reference yield:

: 1616969-91-5
(Z)-5-(4-trifluoromethylbenzylidene)-2-(4-methoxybenzylthio)-4-thiazolidinone

: 1616969-88-0
C₂₃H₂₁F₃N₂O₃S₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium; N-ethyl-N,N-diisopropylamine / tetrahydrofuran; hexane / 0.5 h / -74 °C / Inert atmosphere

1.2: 1 h / Inert atmosphere

2.1: chiralpak IA / hexane; dichloromethane; isopropyl alcohol / Resolution of racemate

3.1: trifluoroacetic acid / 1 h / Reflux

With n-butyllithium; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; hexane; dichloromethane; isopropyl alcohol;
DOI:10.1002/cmdc.201300553