Technology Process of 3,4,5-trihydroxyphenethyl alcohol methylether
There total 5 articles about 3,4,5-trihydroxyphenethyl alcohol methylether which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: carbonic acid dimethyl ester; sodium bromide; potassium peroxymonosulfate / water / 20 °C / Green chemistry
2.1: copper(I) bromide / methanol / 20 °C / Green chemistry
2.2: 3 h / 90 °C / Green chemistry
3.1: boron tribromide / dichloromethane / -40 °C
4.1: amberlyst 15 / methanol / 36 h / Reflux
With
potassium peroxymonosulfate; boron tribromide; carbonic acid dimethyl ester; sodium bromide; copper(I) bromide;
In
methanol; dichloromethane; water;
DOI:10.1007/s00044-012-0052-8
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: copper(I) bromide / methanol / 20 °C / Green chemistry
1.2: 3 h / 90 °C / Green chemistry
2.1: boron tribromide / dichloromethane / -40 °C
3.1: amberlyst 15 / methanol / 36 h / Reflux
With
boron tribromide; copper(I) bromide;
In
methanol; dichloromethane;
DOI:10.1007/s00044-012-0052-8
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: copper(I) bromide; carbonic acid dimethyl ester / methanol / 20 °C / Green chemistry
1.2: 3 h / 90 °C / Green chemistry
2.1: boron tribromide / dichloromethane / -40 °C
3.1: amberlyst 15 / methanol / 36 h / Reflux
With
boron tribromide; carbonic acid dimethyl ester; copper(I) bromide;
In
methanol; dichloromethane;
DOI:10.1007/s00044-012-0052-8
