4-hydroxy-3,5-dimethoxyphenethyl methyl carbonate

Base Information

Chemical Name:4-hydroxy-3,5-dimethoxyphenethyl methyl carbonate
CAS No.:1375102-20-7
Molecular Formula:C₁₂H₁₆O₆
Molecular Weight:256.255
Hs Code.:

Synonyms:4-hydroxy-3,5-dimethoxyphenethyl methyl carbonate

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Chemical Property of 4-hydroxy-3,5-dimethoxyphenethyl methyl carbonate

Chemical Property:

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Technology Process of 4-hydroxy-3,5-dimethoxyphenethyl methyl carbonate

There total 4 articles about 4-hydroxy-3,5-dimethoxyphenethyl methyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1375102-34-3
3,5-dibromo-4-hydroxyphenethyl methyl carbonate

: 124-41-4
sodium methylate

: 1375102-20-7
4-hydroxy-3,5-dimethoxyphenethyl methyl carbonate

Guidance literature:: sodium methylate; With carbonic acid dimethyl ester; copper(I) bromide; In methanol; at 20 ℃; Green chemistry;

3,5-dibromo-4-hydroxyphenethyl methyl carbonate; In methanol; at 90 ℃; for 3h; Green chemistry;
DOI:10.1007/s00044-012-0052-8

Reference yield: 41.0%

: 124-41-4
sodium methylate

: 616-38-6
carbonic acid dimethyl ester

: 2,6-dibromo-4-(2-hydroxy-ethyl)-phenol

: 1375102-20-7
4-hydroxy-3,5-dimethoxyphenethyl methyl carbonate

: 20824-45-7
4-hydroxy-3,5-dimethoxyphenethyl alcohol

Guidance literature:: sodium methylate; carbonic acid dimethyl ester; With copper(I) bromide; In methanol; at 20 ℃; Green chemistry;

2,6-dibromo-4-(2-hydroxy-ethyl)-phenol; In methanol; at 90 ℃; for 3h; Green chemistry;
DOI:10.1007/s00044-012-0052-8

Reference yield:

: 501-94-0
p-hydroxyphenethyl alcohol

: 1375102-20-7
4-hydroxy-3,5-dimethoxyphenethyl methyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: carbonic acid dimethyl ester; sodium bromide; potassium peroxymonosulfate / water / 20 °C / Green chemistry

2.1: copper(I) bromide / methanol / 20 °C / Green chemistry

2.2: 3 h / 90 °C / Green chemistry

With potassium peroxymonosulfate; carbonic acid dimethyl ester; sodium bromide; copper(I) bromide; In methanol; water;
DOI:10.1007/s00044-012-0052-8