3,5-dibromo-4-hydroxyphenethyl methyl carbonate

Base Information

Chemical Name:3,5-dibromo-4-hydroxyphenethyl methyl carbonate
CAS No.:1375102-34-3
Molecular Formula:C₁₀H₁₀Br₂O₄
Molecular Weight:353.995
Hs Code.:

Synonyms:3,5-dibromo-4-hydroxyphenethyl methyl carbonate

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Chemical Property of 3,5-dibromo-4-hydroxyphenethyl methyl carbonate

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Technology Process of 3,5-dibromo-4-hydroxyphenethyl methyl carbonate

There total 2 articles about 3,5-dibromo-4-hydroxyphenethyl methyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 953422-33-8
2-(4'-hydroxyphenyl)ethyl methyl carbonate

: 1375102-34-3
3,5-dibromo-4-hydroxyphenethyl methyl carbonate

Guidance literature:: With potassium peroxymonosulfate; carbonic acid dimethyl ester; sodium bromide; In water; at 20 ℃; Green chemistry;
DOI:10.1007/s00044-012-0052-8

Reference yield:

: 501-94-0
p-hydroxyphenethyl alcohol

: 1375102-34-3
3,5-dibromo-4-hydroxyphenethyl methyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: amberlyst 15 / Reflux; Green chemistry

2: carbonic acid dimethyl ester; sodium bromide; potassium peroxymonosulfate / water / 20 °C / Green chemistry

With potassium peroxymonosulfate; carbonic acid dimethyl ester; sodium bromide; In water;
DOI:10.1007/s00044-012-0052-8

Reference yield: 87.0%

: 1375102-34-3
3,5-dibromo-4-hydroxyphenethyl methyl carbonate

: 124-41-4
sodium methylate

: 1375102-20-7
4-hydroxy-3,5-dimethoxyphenethyl methyl carbonate

Guidance literature:: sodium methylate; With carbonic acid dimethyl ester; copper(I) bromide; In methanol; at 20 ℃; Green chemistry;

3,5-dibromo-4-hydroxyphenethyl methyl carbonate; In methanol; at 90 ℃; for 3h; Green chemistry;
DOI:10.1007/s00044-012-0052-8