Technology Process of C17H13NO6S
There total 5 articles about C17H13NO6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: aluminum (III) chloride / dichloromethane / 3 h / 0 °C
2: sodium hydroxide; water / 4 h / 20 °C
3: acetic anhydride / 24 h / Reflux
With
aluminum (III) chloride; water; acetic anhydride; sodium hydroxide;
In
dichloromethane;
1: |Friedel-Crafts Acylation;
DOI:10.1016/j.bmcl.2014.02.074
- Guidance literature:
-
Multi-step reaction with 2 steps
1: ammonium hydroxide / methanol / 24 h / 20 °C
2: acetic anhydride / 24 h / Reflux
With
ammonium hydroxide; acetic anhydride;
In
methanol;
DOI:10.1016/j.bmcl.2014.02.074
- Guidance literature:
-
Multi-step reaction with 3 steps
1: chlorosulfonic acid / 24 h / 0 - 20 °C
2: ammonium hydroxide / methanol / 24 h / 20 °C
3: acetic anhydride / 24 h / Reflux
With
chlorosulfonic acid; ammonium hydroxide; acetic anhydride;
In
methanol;
DOI:10.1016/j.bmcl.2014.02.074