Technology Process of C66H92N4O19Zn
There total 9 articles about C66H92N4O19Zn which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: triethylamine / dichloromethane
2: potassium carbonate / acetone / Reflux
3: lithium aluminium tetrahydride / tetrahydrofuran
4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane
5: borane tert-butylamine / dichloromethane
6: dichloromethane; methanol
With
dmap; lithium aluminium tetrahydride; borane tert-butylamine; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; acetone;
DOI:10.1246/cl.2012.1689
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane
2: borane tert-butylamine / dichloromethane
3: dichloromethane; methanol
With
dmap; borane tert-butylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
methanol; dichloromethane;
DOI:10.1246/cl.2012.1689
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium carbonate / acetone / Reflux
2: lithium aluminium tetrahydride / tetrahydrofuran
3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane
4: borane tert-butylamine / dichloromethane
5: dichloromethane; methanol
With
dmap; lithium aluminium tetrahydride; borane tert-butylamine; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran; methanol; dichloromethane; acetone;
DOI:10.1246/cl.2012.1689