Technology Process of C23H31NSi
There total 9 articles about C23H31NSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Amberlyst A21 / dichloromethane / 1 h
2: tetrahydrofuran; hexane / 0.17 h
With
Amberlyst A21;
In
tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/jo200991q
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sec.-butyllithium; (-)-sparteine / diethyl ether / 5.5 h / -78 °C / Inert atmosphere
1.2: 0.5 h / -78 - 20 °C / Inert atmosphere
2.1: water; zinc dibromide / dichloromethane / 16 h
3.1: Amberlyst A21 / dichloromethane / 1 h
4.1: tetrahydrofuran; hexane / 0.17 h
With
water; sec.-butyllithium; zinc dibromide; (-)-sparteine;
In
tetrahydrofuran; diethyl ether; hexane; dichloromethane;
DOI:10.1021/jo200991q
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: ammonium hexafluorosilicate / 1,2-dimethoxyethane / 120 h / Inert atmosphere; Reflux
2.1: sec.-butyllithium; (-)-sparteine / diethyl ether / 5.5 h / -78 °C / Inert atmosphere
2.2: 0.5 h / -78 - 20 °C / Inert atmosphere
3.1: water; zinc dibromide / dichloromethane / 16 h
4.1: Amberlyst A21 / dichloromethane / 1 h
5.1: tetrahydrofuran; hexane / 0.17 h
With
ammonium hexafluorosilicate; water; sec.-butyllithium; zinc dibromide; (-)-sparteine;
In
tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; hexane; dichloromethane;
DOI:10.1021/jo200991q
