Technology Process of C22H25N5O4S2
There total 5 articles about C22H25N5O4S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 65 - 120 °C
2: palladium on activated charcoal; hydrogen / tetrahydrofuran; ethanol / 50 °C
3: ethanol / Reflux
4: hydrogenchloride / water; 1,4-dioxane; dichloromethane
5: N-ethyl-N,N-diisopropylamine / tetrahydrofuran
With
hydrogenchloride; palladium on activated charcoal; hydrogen; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; isopropyl alcohol;
DOI:10.1016/j.bmcl.2012.10.008
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogenchloride / water; 1,4-dioxane; dichloromethane
2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran
With
hydrogenchloride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1016/j.bmcl.2012.10.008
- Guidance literature:
-
Multi-step reaction with 4 steps
1: palladium on activated charcoal; hydrogen / tetrahydrofuran; ethanol / 50 °C
2: ethanol / Reflux
3: hydrogenchloride / water; 1,4-dioxane; dichloromethane
4: N-ethyl-N,N-diisopropylamine / tetrahydrofuran
With
hydrogenchloride; palladium on activated charcoal; hydrogen; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water;
DOI:10.1016/j.bmcl.2012.10.008