1-n-butyl-2,3-dimethylimidazolium [N,N'-bis(2,4,6-trimethyl-3-sulfonatophenyl)butane-2,3-diimine-κ2N,N'][η2:η2-(Z,Z)-cycloocta-1.5-diene]rhodium(I)

Base Information

• Chemical Name: 1-n-butyl-2,3-dimethylimidazolium [N,N'-bis(2,4,6-trimethyl-3-sulfonatophenyl)butane-2,3-diimine-κ2N,N'][η2:η2-(Z,Z)-cycloocta-1.5-diene]rhodium(I)
• CAS No.: 1350897-96-9
• Molecular Formula: C₉H₁₇N₂*C₃₀H₃₈N₂O₆RhS₂
• Molecular Weight: 842.926

Synonyms:

Chemical Property of 1-n-butyl-2,3-dimethylimidazolium [N,N'-bis(2,4,6-trimethyl-3-sulfonatophenyl)butane-2,3-diimine-κ2N,N'][η2:η2-(Z,Z)-cycloocta-1.5-diene]rhodium(I)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 1-n-butyl-2,3-dimethylimidazolium [N,N'-bis(2,4,6-trimethyl-3-sulfonatophenyl)butane-2,3-diimine-κ2N,N'][η2:η2-(Z,Z)-cycloocta-1.5-diene]rhodium(I)

There total 1 articles about 1-n-butyl-2,3-dimethylimidazolium [N,N'-bis(2,4,6-trimethyl-3-sulfonatophenyl)butane-2,3-diimine-κ2N,N'][η2:η2-(Z,Z)-cycloocta-1.5-diene]rhodium(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

silver tetrafluoroborate (14104-20-2) + chloro(1,5-cyclooctadiene)rhodium(I) dimer + bis(1-n-butyl-2,3-dimethylimidazolium) N,N'-bis(2,4,6-trimethyl-3-sulfonatophenyl)butane-2,3-diimine → 1-n-butyl-2,3-dimethylimidazolium [N,N'-bis(2,4,6-trimethyl-3-sulfonatophenyl)butane-2,3-diimine-κ2N,N'][η2:η2-(Z,Z)-cycloocta-1.5-diene]rhodium(I) (1350897-96-9)

Guidance literature:

In acetonitrile; byproducts: AgCl; (Schlenk or glovebox); mixt. of AgBF4 and Rh-complex stirred in MeCN for1 h at room temp., filtered, added to soln. of ligand in MeCN, stirred for 1 h at room temp.; volatiles removed in vacuo, treated with CH2Cl2-ether 1:1, filtered, washed with ether, dried at 1E-2 mbar;

DOI:10.1039/c1dt10939a

upstream raw materials:

silver tetrafluoroborate

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