C₄₃H₆₆N₄O₁₀Si₂

Base Information

Chemical Name:C₄₃H₆₆N₄O₁₀Si₂
CAS No.:1355340-80-5
Molecular Formula:C₄₃H₆₆N₄O₁₀Si₂
Molecular Weight:855.189
Hs Code.:

C<sub>43</sub>H<sub>66</sub>N<sub>4</sub>O<sub>10</sub>Si<sub>2</sub>

Synonyms:

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Chemical Property of C₄₃H₆₆N₄O₁₀Si₂

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Technology Process of C₄₃H₆₆N₄O₁₀Si₂

There total 8 articles about C₄₃H₆₆N₄O₁₀Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₂H₆₁N₃O₁₁Si₂

: 74-89-5
methylamine

: 1355340-80-5
C₄₃H₆₆N₄O₁₀Si₂

Guidance literature:: C₄₂H₆₁N₃O₁₁Si₂; methylamine; With sodium tris(acetoxy)borohydride; acetic acid; In tetrahydrofuran; ethyl acetate; at 25 ℃; for 48h; Molecular sieve; Inert atmosphere;

With sodium hydrogencarbonate; In tetrahydrofuran; water; ethyl acetate; Inert atmosphere;
DOI:10.1021/jo202061t

Reference yield:

: 1355340-61-2
C₂₃H₄₂N₂O₇Si₂

: 1355340-80-5
C₄₃H₆₆N₄O₁₀Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / water; acetonitrile / 0.67 h / 25 °C / Inert atmosphere

2.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

3.1: methanol / dichloromethane / 4 h / 0 °C / Inert atmosphere

3.2: 0.08 h / 20 °C / Inert atmosphere

4.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 0 °C / Inert atmosphere

5.1: sodium tris(acetoxy)borohydride; acetic acid / tetrahydrofuran; ethyl acetate / 48 h / 25 °C / Molecular sieve; Inert atmosphere

5.2: Inert atmosphere

With methanol; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; sodium tris(acetoxy)borohydride; sodium hydrogencarbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; Dess-Martin periodane; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo202061t

Reference yield:

: 1355340-62-3
C₂₃H₄₀N₂O₈Si₂

: 1355340-80-5
C₄₃H₆₆N₄O₁₀Si₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

2.1: methanol / dichloromethane / 4 h / 0 °C / Inert atmosphere

2.2: 0.08 h / 20 °C / Inert atmosphere

3.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 0 °C / Inert atmosphere

4.1: sodium tris(acetoxy)borohydride; acetic acid / tetrahydrofuran; ethyl acetate / 48 h / 25 °C / Molecular sieve; Inert atmosphere

4.2: Inert atmosphere

With methanol; sodium tris(acetoxy)borohydride; sodium hydrogencarbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; Dess-Martin periodane; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jo202061t