C₁₂H₁₄ClNO₃S

Base Information

Chemical Name:C₁₂H₁₄ClNO₃S
CAS No.:1509935-66-3
Molecular Formula:C₁₂H₁₄ClNO₃S
Molecular Weight:287.767
Hs Code.:

C<sub>12</sub>H<sub>14</sub>ClNO<sub>3</sub>S

Synonyms:

Suppliers and Price of C₁₂H₁₄ClNO₃S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₁₄ClNO₃S

Chemical Property:

Purity/Quality:

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Technology Process of C₁₂H₁₄ClNO₃S

There total 4 articles about C₁₂H₁₄ClNO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1509935-56-1
C₁₉H₂₁NOS

: 1509935-66-3
C₁₂H₁₄ClNO₃S

Guidance literature:: With sulfuryl dichloride; acetic acid; In dichloromethane; water; at 0 - 20 ℃; for 1.58333h;
DOI:10.1021/jm4005835

Reference yield:

: 108-36-1
1,3-dibromobenzene

: 1509935-66-3
C₁₂H₁₄ClNO₃S

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium diisopropyl amide / tetrahydrofuran; n-heptane; ethylbenzene / 2.75 h / -78 - -65 °C

2.1: n-butyllithium; sulfur / tetrahydrofuran; n-heptane / 0.75 h / -78 °C / Inert atmosphere

2.2: 1.5 h / -78 °C / Inert atmosphere

3.1: potassium carbonate; copper(l) iodide; N,N,N,N,-tetramethylethylenediamine / toluene / 20 h / 110 °C / Inert atmosphere

4.1: acetic acid; sulfuryl dichloride / water; dichloromethane / 1.58 h / 0 - 20 °C

With copper(l) iodide; n-butyllithium; sulfuryl dichloride; N,N,N,N,-tetramethylethylenediamine; potassium carbonate; sulfur; acetic acid; lithium diisopropyl amide; In tetrahydrofuran; n-heptane; dichloromethane; ethylbenzene; water; toluene;
DOI:10.1021/jm4005835

Reference yield:

: 69321-60-4
2,6-dibromotoluene

: 1509935-66-3
C₁₂H₁₄ClNO₃S

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium; sulfur / tetrahydrofuran; n-heptane / 0.75 h / -78 °C / Inert atmosphere

1.2: 1.5 h / -78 °C / Inert atmosphere

2.1: potassium carbonate; copper(l) iodide; N,N,N,N,-tetramethylethylenediamine / toluene / 20 h / 110 °C / Inert atmosphere

3.1: acetic acid; sulfuryl dichloride / water; dichloromethane / 1.58 h / 0 - 20 °C

With copper(l) iodide; n-butyllithium; sulfuryl dichloride; N,N,N,N,-tetramethylethylenediamine; potassium carbonate; sulfur; acetic acid; In tetrahydrofuran; n-heptane; dichloromethane; water; toluene;
DOI:10.1021/jm4005835