diphenyl ferrocenylmethylphosphonate

Base Information

Chemical Name:diphenyl ferrocenylmethylphosphonate
CAS No.:174811-35-9
Molecular Formula:C₂₃H₂₁FeO₃P
Molecular Weight:432.239
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diphenyl ferrocenylmethylphosphonate

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Technology Process of diphenyl ferrocenylmethylphosphonate

There total 1 articles about diphenyl ferrocenylmethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 101-02-0
triphenyl phosphite

: 1273-86-5
1-ferrocenylmethanol

: 174811-35-9
diphenyl ferrocenylmethylphosphonate

Guidance literature:: In neat (no solvent); heating (130°C, 15 min), cooling (room temp.), dissolution (petroleum spirit), stirring (5 min), cooling (-18°C, overnight), decantation, petroleum spirit addn., stirring (room temp., crystn.); washing (cold petroleum spirit, drying in vacuum; elem. anal.;
DOI:10.1016/0277-5387(95)00347-9

Reference yield: 4.6%

: 174811-35-9
diphenyl ferrocenylmethylphosphonate

: 1333-74-0
hydrogen

: 399043-59-5
C₅H₅FeC₅H₄CH₂P(O)(OC₆H₅)(OH)

Guidance literature:: platinum(IV) oxide; In methanol; stirring a mixt. of PtO2 and iron complex in methanol under H2 for 4 d; slow evapn., dissolving in CH2Cl2, extn. with aq. NaHCO3, washing with CH2Cl2, addn. of concd. HCl, extn. with CH2Cl2, drying (MgSO4), filtration, addn. of petroleum ether, filtration, drying in air; elem. anal.;
DOI:10.1016/S0022-328X(01)00908-1