C₃₉H₂₉ClO

Base Information

• Chemical Name: C₃₉H₂₉ClO
• CAS No.: 1541181-14-9
• Molecular Formula: C₃₉H₂₉ClO
• Molecular Weight: 549.112
• Mol file: 1541181-14-9.mol

Synonyms:

Chemical Property of C₃₉H₂₉ClO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₉H₂₉ClO

There total 3 articles about C₃₉H₂₉ClO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C39H30O2 (318293-78-6) → C39H29ClO (1541181-14-9)

Guidance literature:

With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃;

DOI:10.1021/ja411379e

Reference yield:

Tris(4-biphenylyl)methanol (5341-14-0) → C39H29ClO (1541181-14-9)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic anhydride; acetic acid / 1.5 h / 110 °C

2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 20 °C

With oxalyl dichloride; acetic anhydride; acetic acid; N,N-dimethyl-formamide; In dichloromethane;

DOI:10.1021/ja411379e

Reference yield:

4-bromo-1,1'-biphenyl (92-66-0) → C39H29ClO (1541181-14-9)

Guidance literature:

Multi-step reaction with 3 steps

1: n-butyllithium / tetrahydrofuran; pentane / 1 h / -78 - 20 °C / Inert atmosphere

2: acetic anhydride; acetic acid / 1.5 h / 110 °C

3: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 20 °C

With n-butyllithium; oxalyl dichloride; acetic anhydride; acetic acid; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; pentane;

DOI:10.1021/ja411379e

upstream raw materials:

Tris(4-biphenylyl)methanol

4-bromo-1,1'-biphenyl

C₃₉H₃₀O₂

Downstream raw materials:

C₈₄H₇₀N₂O₄