(thiosalicylato)zinc

Base Information

Chemical Name:(thiosalicylato)zinc
CAS No.:36301-51-6
Molecular Formula:C₇H₄O₂S*Zn
Molecular Weight:217.564
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (thiosalicylato)zinc

Chemical Property:

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Technology Process of (thiosalicylato)zinc

There total 2 articles about (thiosalicylato)zinc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.3%

: 56-34-8
tetraethylammonium chloride

: 5970-45-6
zinc(II) acetate dihydrate

: 147-93-3
Thiosalicylic acid

: N(C₂H₅)4⁽¹⁺⁾*Na⁽¹⁺⁾*Zn⁽²⁺⁾*2SC₆H₄COO^(2-)*H₂O=N(C₂H₅)4NaZn(SC₆H₄COO)2*H₂O

: 36301-51-6
(thiosalicylato)zinc

Guidance literature:: With NaCH₃COO; In ethanol; to soln. of ligand in EtOH was added suspn. of NaCH3COO in EtOH, soln. of Zn-salt in warm EtOH was added with stirring under N2; filtered, washed with warm EtOH and ether, dried, NEt4Cl in EtOH was added to filtrate, sepd., solvent was removed by vac., filtered, washed with ether, dried; elem. anal.;
DOI:10.1021/ic000223q

Reference yield: 22.0%

: 147-93-3
Thiosalicylic acid

: 7646-85-7,24359-56-6
zinc(II) chloride

: 36301-51-6
(thiosalicylato)zinc

Guidance literature:: With KOH; In water; a soln. of ZnCl2 added to a rapidly stirred soln. of thiosalicylic acid and KOH, heated for 18 h at 210°C in an autoclave, cooled slowly; decanted with H2O, filtered and dried, crystals isolated manually under a light microscope, washed in hexane; elem. anal.;
DOI:10.1039/b401887g