C₃₁H₃₂N₂O₅S

Base Information

Chemical Name:C₃₁H₃₂N₂O₅S
CAS No.:113352-70-8
Molecular Formula:C₃₁H₃₂N₂O₅S
Molecular Weight:544.671
Hs Code.:

C<sub>31</sub>H<sub>32</sub>N<sub>2</sub>O<sub>5</sub>S

Synonyms:

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Chemical Property of C₃₁H₃₂N₂O₅S

Chemical Property:

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Technology Process of C₃₁H₃₂N₂O₅S

There total 14 articles about C₃₁H₃₂N₂O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 113352-69-5
C₃₁H₃₂N₂O₄S

: 113352-70-8,113429-12-2,113773-83-4,113773-84-5
C₃₁H₃₂N₂O₅S

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1016/S0040-4039(00)95497-2

Reference yield:

: 113352-66-2
1-(4-methoxy-2-nitrophenyl)propan-2-one

: 113352-70-8,113429-12-2,113773-83-4,113773-84-5
C₃₁H₃₂N₂O₅S

Guidance literature:: Multi-step reaction with 6 steps

1: 95 percent / H₂ / Raney-Ni / ethyl acetate / 18 h

2: 84 percent / POCl₃ / 0.5 h / 0 °C

3: 79 percent / NaH / tetrahydrofuran / 0.25 h / from 0 deg C to room temp.

4: 100 percent / molecular sieves (3 Angstroem) / toluene / 23 h / 20 °C

5: 64 percent / diisopropylethylamine / toluene / 1 h / Heating

6: 98 percent / MCPBA, 10percent Na₂CO₃ / CH₂Cl₂; H₂O / 1 h / 0 °C

With 3 A molecular sieve; hydrogen; sodium hydride; sodium carbonate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; trichlorophosphate; nickel; In tetrahydrofuran; dichloromethane; water; ethyl acetate; toluene;
DOI:10.1021/ja00215a039

Reference yield:

: 4-Methoxy-2-nitro-benzenediazonium; hydrogen sulfate

: 113352-70-8,113429-12-2,113773-83-4,113773-84-5
C₃₁H₃₂N₂O₅S

Guidance literature:: Multi-step reaction with 7 steps

1: 55 percent / 0.5M HCl, LiCl / CuCl / H₂O; various solvent(s) / 5 deg C, 3.5 h. then 20 deg C, 4 h.

2: 95 percent / H₂ / Raney-Ni / ethyl acetate / 18 h

3: 84 percent / POCl₃ / 0.5 h / 0 °C

4: 79 percent / NaH / tetrahydrofuran / 0.25 h / from 0 deg C to room temp.

5: 100 percent / molecular sieves (3 Angstroem) / toluene / 23 h / 20 °C

6: 64 percent / diisopropylethylamine / toluene / 1 h / Heating

7: 98 percent / MCPBA, 10percent Na₂CO₃ / CH₂Cl₂; H₂O / 1 h / 0 °C

With hydrogenchloride; 3 A molecular sieve; hydrogen; sodium hydride; sodium carbonate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium chloride; trichlorophosphate; nickel; copper(l) chloride; In tetrahydrofuran; dichloromethane; water; ethyl acetate; toluene;
DOI:10.1021/ja00215a039