1,4-bis-diphenylphosphanyl-[1,4]diazepane

Base Information

• Chemical Name: 1,4-bis-diphenylphosphanyl-[1,4]diazepane
• CAS No.: 476172-53-9
• Molecular Formula: C₂₉H₃₀N₂P₂
• Molecular Weight: 468.518

Synonyms:

Chemical Property of 1,4-bis-diphenylphosphanyl-[1,4]diazepane

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 1,4-bis-diphenylphosphanyl-[1,4]diazepane

There total 1 articles about 1,4-bis-diphenylphosphanyl-[1,4]diazepane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,4-Diazacycloheptane (505-66-8) + chloro-diphenylphosphine (1079-66-9,74391-44-9) → 1,4-bis-diphenylphosphanyl-[1,4]diazepane (476172-53-9)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃;

DOI:10.1080/10426500108546604

Reference yield: 92.0%

dichloro( 1,5-cyclooctadiene)platinum(ll) (12080-32-9) + 1,4-bis-diphenylphosphanyl-[1,4]diazepane (476172-53-9) → cis-[PtCl2((C6H5)2PN(C5H10)NP(C6H5)2)] (476172-55-1)

Guidance literature:

In dichloromethane; 1:1 mixt. stirred for 2 h, concd.; pptd. (Et2O), filtered off, elem. anal.;

DOI:10.1016/S0277-5387(02)01007-0

Reference yield: 87.0%

dichloro(1,5-cyclooctadiene)palladium(II) (12107-56-1) + 1,4-bis-diphenylphosphanyl-[1,4]diazepane (476172-53-9) → cis-[PdCl2((C6H5)2PN(C5H10)NP(C6H5)2)] (476172-57-3)

Guidance literature:

In dichloromethane; 1:1 mixt. stirred for 2 h, concd.; pptd. (Et2O), filtered off, elem. anal.;

DOI:10.1016/S0277-5387(02)01007-0

upstream raw materials:

1,4-Diazacycloheptane

chloro-diphenylphosphine

Downstream raw materials:

Mo(CO)4(((C₆H₅)2PN)2(CH₂)2(CH₂)3)

cis-[PdCl₂((C₆H₅)2PN(C₅H₁₀)NP(C₆H₅)2)]

[(C₆H₅)2P(AuCl)N(C₅H₁₀)N(AuCl)P(C₆H₅)2]

cis-[Pt(CH₃)2((C₆H₅)2PN(C₅H₁₀)NP(C₆H₅)2)]

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