C₈₀H₈₆O₁₉

Base Information

Chemical Name:C₈₀H₈₆O₁₉
CAS No.:124814-09-1
Molecular Formula:C₈₀H₈₆O₁₉
Molecular Weight:1351.55
Hs Code.:

C<sub>80</sub>H<sub>86</sub>O<sub>19</sub>

Synonyms:

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Chemical Property of C₈₀H₈₆O₁₉

Chemical Property:

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Technology Process of C₈₀H₈₆O₁₉

There total 13 articles about C₈₀H₈₆O₁₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 97590-76-6
benzyl-O-β-D-glucopyranoside

: 124814-09-1
C₈₀H₈₆O₁₉

Guidance literature:: Multi-step reaction with 10 steps

1: NaOAc / 4 h / 110 °C

2: 69.3 percent / 1.) crushed molecular sieves (4 Angstroem); 2.) trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 1.) r.t., 0.5 h; 2.) -20 deg C to r.t.

3: 1percent NaOMe / methanol / Ambient temperature

4: ZnCl₂ / Ambient temperature

5: NaH (60percent dispersion in oil) / dimethylformamide / -30 °C

6: toluene / Heating

7: 95 percent / Na / methanol; dioxane / Ambient temperature

8: 94 percent / NaH (60percent dispersion in oil) / dimethylformamide / 1 h / Ambient temperature

9: 62 percent / sodium cyanoborohydride, HCl, crushed molecular sieves (4 Angstroem) / diethyl ether; tetrahydrofuran / 0.5 h / 0 °C

10: 1.) crushed molecular sieves (4 Angstroem); 2.) trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 1.) r.t., 0.5 h; 2.) -20 deg C to r.t.

With hydrogenchloride; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; sodium methylate; sodium acetate; sodium; sodium hydride; sodium cyanoborohydride; zinc(II) chloride; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/0008-6215(89)84070-4

Reference yield:

: 582-52-5
1,2:5,6-di-O-isopropylidene-α-D-glucofuranose

: 124814-09-1
C₈₀H₈₆O₁₉

Guidance literature:: Multi-step reaction with 11 steps

1: 1.) NaH (60percent dispersion in oil); 2.) 60percent aq. acetic acid; 3.) 0.1M H₂SO₄ / 1.) DMF, 90 deg C, 2 h; 2.) 90 deg C, 2 h; 3.) 90 deg C, 2 h

2: NaOAc / 4 h / 110 °C

3: 69.3 percent / 1.) crushed molecular sieves (4 Angstroem); 2.) trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 1.) r.t., 0.5 h; 2.) -20 deg C to r.t.

4: 1percent NaOMe / methanol / Ambient temperature

5: ZnCl₂ / Ambient temperature

6: NaH (60percent dispersion in oil) / dimethylformamide / -30 °C

7: toluene / Heating

8: 95 percent / Na / methanol; dioxane / Ambient temperature

9: 94 percent / NaH (60percent dispersion in oil) / dimethylformamide / 1 h / Ambient temperature

10: 62 percent / sodium cyanoborohydride, HCl, crushed molecular sieves (4 Angstroem) / diethyl ether; tetrahydrofuran / 0.5 h / 0 °C

11: 1.) crushed molecular sieves (4 Angstroem); 2.) trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 1.) r.t., 0.5 h; 2.) -20 deg C to r.t.

With hydrogenchloride; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; sulfuric acid; sodium methylate; sodium acetate; sodium; sodium hydride; sodium cyanoborohydride; acetic acid; zinc(II) chloride; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/0008-6215(89)84070-4

Reference yield:

: 100-39-0
benzyl bromide

: 124814-09-1
C₈₀H₈₆O₁₉

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH (60percent dispersion in oil); 2.) 60percent aq. acetic acid; 3.) 0.1M H₂SO₄ / 1.) DMF, 90 deg C, 2 h; 2.) 90 deg C, 2 h; 3.) 90 deg C, 2 h

2: NaOAc / 4 h / 110 °C

3: 1.) crushed molecular sieves (4 Angstroem); 2.) trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 1.) r.t., 0.5 h; 2.) -20 deg C to r.t.

With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; sulfuric acid; sodium acetate; sodium hydride; acetic acid; In dichloromethane;
DOI:10.1016/0008-6215(89)84070-4