1-deoxy-1--β-D-glucopyranose

Base Information

Chemical Name:1-deoxy-1--β-D-glucopyranose
CAS No.:161761-59-7
Molecular Formula:C₁₉H₃₀N₂O₆S
Molecular Weight:414.523
Hs Code.:

1-deoxy-1-<p-(6-aminohexanamido)benzylthio>-β-D-glucopyranose

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-deoxy-1--β-D-glucopyranose

Chemical Property:

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Technology Process of 1-deoxy-1--β-D-glucopyranose

There total 5 articles about 1-deoxy-1--β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 161761-58-6
Acetic acid (2R,3R,4S,5R,6S)-3,5-diacetoxy-2-acetoxymethyl-6-{4-[6-(2,2,2-trifluoro-acetylamino)-hexanoylamino]-benzylsulfanyl}-tetrahydro-pyran-4-yl ester

: 161761-59-7
1-deoxy-1--β-D-glucopyranose

Guidance literature:: With ethanol; AV-17 ionexchange resin; for 6h; Ambient temperature;

Reference yield:

: 19879-84-6
tetraacetyl thioglucose

: 161761-59-7
1-deoxy-1--β-D-glucopyranose

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / K₂CO₃ / acetone; H₂O / 1 h / Ambient temperature

2: 93 percent / aq. CaCl₂, Zn, 78percent aq. EtOH / 2 h / Heating

3: dicyclohexylcarbodiimide, pyridine / a) 4 deg C, 4 h, b) 20 deg C, 5 d

4: 72 percent / 67percent aq. EtOH, AV-17 ionexchange resin / 6 h / Ambient temperature

With pyridine; ethanol; AV-17 ionexchange resin; potassium carbonate; dicyclohexyl-carbodiimide; calcium chloride; zinc; In water; acetone;

Reference yield:

: 407-91-0
6-(trifluoroacetamido)hexanoic acid

: 161761-59-7
1-deoxy-1--β-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexylcarbodiimide, pyridine / a) 4 deg C, 4 h, b) 20 deg C, 5 d

2: 72 percent / 67percent aq. EtOH, AV-17 ionexchange resin / 6 h / Ambient temperature

With pyridine; ethanol; AV-17 ionexchange resin; dicyclohexyl-carbodiimide;