((R)-(-)-3,5-di-tert-butyl-4-methoxy-segphos)CuH

Base Information

• Chemical Name: ((R)-(-)-3,5-di-tert-butyl-4-methoxy-segphos)CuH
• CAS No.: 478044-08-5
• Molecular Formula: C₇₄H₁₀₁CuO₈P₂
• Molecular Weight: 1244.1
• Mol file: 478044-08-5.mol

Synonyms:

Chemical Property of ((R)-(-)-3,5-di-tert-butyl-4-methoxy-segphos)CuH

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of ((R)-(-)-3,5-di-tert-butyl-4-methoxy-segphos)CuH

There total 1 articles about ((R)-(-)-3,5-di-tert-butyl-4-methoxy-segphos)CuH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-(-)-3,5-di-tert-butyl-4-methoxy-segphos (210169-40-7,566940-03-2,638196-78-8) + copper(II) acetate monohydrate (6046-93-1) → ((R)-(-)-3,5-di-tert-butyl-4-methoxy-segphos)CuH (872517-04-9,478044-08-5)

Guidance literature:

With polymethylhydrosiloxane; In toluene; oven-dried poly-coated amber glass bottle equipped with stirrer bar purged under Ar, under inert atmosphere (glovebox) Cu(OAc)2 and segphos added followed by dry toluene, mixt. stirred for 2 h at room temp., siloxaneadded dropwise, stirred for 30 min;

DOI:10.1002/anie.200500800

upstream raw materials:

(R)-(-)-3,5-di-tert-butyl-4-methoxy-segphos

copper(II) acetate monohydrate