1H-Pyrrolo[1,2-a]imidazole-5,7-dicarboxylic acid, 1-[2-[(3-ethoxy-3-oxo-1-propenyl)thio]-1-phenylethenyl]-2,3-dihydro-, diethyl ester, (Z,Z)-

Base Information

• Chemical Name: 1H-Pyrrolo[1,2-a]imidazole-5,7-dicarboxylic acid, 1-[2-[(3-ethoxy-3-oxo-1-propenyl)thio]-1-phenylethenyl]-2,3-dihydro-, diethyl ester, (Z,Z)-
• CAS No.: 139313-23-8
• Molecular Formula: C₂₅H₂₈N₂O₆S
• Molecular Weight: 484.573

Synonyms:

Chemical Property of 1H-Pyrrolo[1,2-a]imidazole-5,7-dicarboxylic acid, 1-[2-[(3-ethoxy-3-oxo-1-propenyl)thio]-1-phenylethenyl]-2,3-dihydro-, diethyl ester, (Z,Z)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 1H-Pyrrolo[1,2-a]imidazole-5,7-dicarboxylic acid, 1-[2-[(3-ethoxy-3-oxo-1-propenyl)thio]-1-phenylethenyl]-2,3-dihydro-, diethyl ester, (Z,Z)-

There total 1 articles about 1H-Pyrrolo[1,2-a]imidazole-5,7-dicarboxylic acid, 1-[2-[(3-ethoxy-3-oxo-1-propenyl)thio]-1-phenylethenyl]-2,3-dihydro-, diethyl ester, (Z,Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-phenyl-7-(2-ethoxy-2-oxoethyl)-5,6-dihydroimidazo<2,1-b>thiazolium bromide (139313-10-3) + propynoic acid ethyl ester (623-47-2) → ethyl (2Z,5Z)-6-<5,7-bis(ethoxycarbonyl)-2,3-dihydro-1H-pyrrolo<1,2-a>imidazol-1-yl>-6-phenyl-4-thiahexa-2,5-dienoate (139313-23-8) + ethyl (2E,5Z)-6-<5,7-bis(ethoxycarbonyl)-2,3-dihydro-1H-pyrrolo<1,2-a>imidazol-1-yl>-6-phenyl-4-thiahexa-2,5-dienoate (139313-24-9)

Guidance literature:

With triethylamine; In acetonitrile; at 20 ℃; for 2h; Yield given. Yields of byproduct given;

DOI:10.1021/jo00034a029

upstream raw materials:

3-phenyl-7-(2-ethoxy-2-oxoethyl)-5,6-dihydroimidazo<2,1-b>thiazolium bromide

propynoic acid ethyl ester

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