4,5-Dichlorophthalic acid monomethylamide

Base Information

• Chemical Name: 4,5-Dichlorophthalic acid monomethylamide
• CAS No.: 86611-82-7
• Molecular Formula: C₉H₇Cl₂NO₃
• Molecular Weight: 248.065
• Mol file: 86611-82-7.mol

Synonyms:

Chemical Property of 4,5-Dichlorophthalic acid monomethylamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4,5-Dichlorophthalic acid monomethylamide

There total 2 articles about 4,5-Dichlorophthalic acid monomethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,5-dichlorophthalic acid (56962-08-4) → 4,5-Dichlorophthalic acid monomethylamide (86611-82-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 96 percent / Acetic anhydride / 5 h / 165 °C

2: H₂O

With acetic anhydride; In water;

DOI:10.1021/jo00166a009

Reference yield:

4,5-dichlorophthalic anhydride (942-06-3) + methylamine (74-89-5) → 4,5-Dichlorophthalic acid monomethylamide (86611-82-7)

Guidance literature:

In water;

DOI:10.1021/jo00166a009

upstream raw materials:

4,5-dichlorophthalic anhydride

methylamine

4,5-dichlorophthalic acid