2-(p-methoxybenzylamino)-2-p-methoxyphenylcyclohexanone

Base Information

• Chemical Name: 2-(p-methoxybenzylamino)-2-p-methoxyphenylcyclohexanone
• CAS No.: 1383927-85-2
• Molecular Formula: C₂₁H₂₅NO₃
• Molecular Weight: 339.434
• Mol file: 1383927-85-2.mol

Synonyms:

Chemical Property of 2-(p-methoxybenzylamino)-2-p-methoxyphenylcyclohexanone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(p-methoxybenzylamino)-2-p-methoxyphenylcyclohexanone

There total 3 articles about 2-(p-methoxybenzylamino)-2-p-methoxyphenylcyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

C21H25NO2 (1383927-88-5) → 2-(p-methoxybenzylamino)-2-p-methoxyphenylcyclohexanone (1383927-85-2)

Guidance literature:

With decalin; at 190 ℃; for 4h;

DOI:10.2174/157340612800493683

Reference yield:

4-methoxybenzonitrile (874-90-8) → 2-(p-methoxybenzylamino)-2-p-methoxyphenylcyclohexanone (1383927-85-2)

Guidance literature:

Multi-step reaction with 4 steps

1: iodine; magnesium / diethyl ether

2: bromine / tetrachloromethane / 0 °C

3: benzene / 120 h / 20 °C

4: decalin / 4 h / 190 °C

With bromine; iodine; magnesium; decalin; In tetrachloromethane; diethyl ether; benzene;

DOI:10.2174/157340612800493683

Reference yield:

para-methylbenzylamine (104-84-7) → 2-(p-methoxybenzylamino)-2-p-methoxyphenylcyclohexanone (1383927-85-2)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene / 120 h / 20 °C

2: decalin / 4 h / 190 °C

With decalin; In benzene;

DOI:10.2174/157340612800493683

upstream raw materials:

C₂₁H₂₅NO₂

4-methoxybenzonitrile

para-methylbenzylamine