6,7-dihydro-3-methyl-2-phenyl-5H-2aλ⁴-thia-1,2,3-triazacyclopentindene

Base Information

• Chemical Name: 6,7-dihydro-3-methyl-2-phenyl-5H-2aλ⁴-thia-1,2,3-triazacyclopentindene
• CAS No.: 71492-10-9
• Molecular Formula: C₁₄H₁₅N₃S
• Molecular Weight: 257.359

Synonyms:

Chemical Property of 6,7-dihydro-3-methyl-2-phenyl-5H-2aλ⁴-thia-1,2,3-triazacyclopentindene

Chemical Property:

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Technology Process of 6,7-dihydro-3-methyl-2-phenyl-5H-2aλ⁴-thia-1,2,3-triazacyclopentindene

There total 6 articles about 6,7-dihydro-3-methyl-2-phenyl-5H-2aλ⁴-thia-1,2,3-triazacyclopentindene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

(Z)-7-chloromethylene-4,5,6,7-tetrahydro-2-phenyl-benz<1,2,3>thiadiazolylium phosphorodichloridate → 6,7-dihydro-3-methyl-2-phenyl-5H-2aλ4-thia-1,2,3-triazacyclopentindene (71492-10-9) + 6,7-dihydro-2-phenyl-5H-2aλ4,3-dithia-1,2-diazacyclopentindene (59008-74-1)

Guidance literature:

With methylamine; In N,N-dimethyl-formamide; for 0.166667h; Ambient temperature;

Reference yield:

methylamine (74-89-5) + 6,7-dihydro-2-phenyl-5H-2aλ4,3-dithia-1,2-diazacyclopentindene (59008-74-1) → 6,7-dihydro-3-methyl-2-phenyl-5H-2aλ4-thia-1,2,3-triazacyclopentindene (71492-10-9)

Guidance literature:

In ethanol; N,N-dimethyl-formamide; at 60 ℃; for 3h;

DOI:10.1039/P19790000926

Reference yield:

(Z)-7-chloromethylene-4,5,6,7-tetrahydro-2-phenyl-benz<1,2,3>thiadiazolylium phosphorodichloridate + methylamine (74-89-5) → 6,7-dihydro-3-methyl-2-phenyl-5H-2aλ4-thia-1,2,3-triazacyclopentindene (71492-10-9) + 6,7-dihydro-2-phenyl-5H-2aλ4,3-dithia-1,2-diazacyclopentindene (59008-74-1)

Guidance literature:

In water; N,N-dimethyl-formamide; for 0.166667h; Ambient temperature;

upstream raw materials:

methylamine

6,7-dihydro-2-phenyl-5H-2aλ⁴,3-dithia-1,2-diazacyclopentindene

Downstream raw materials:

2,3-diphenyl-3,5,6,7-tetrahydro-2H-2aλ⁴-thia-1,2,3,4-tetraaza-cyclopenta[cd]indene

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