Technology Process of 2-<2,5-dimethoxybenzyl>-3-methoxybenzoic acid
There total 12 articles about 2-<2,5-dimethoxybenzyl>-3-methoxybenzoic acid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 65 percent / Amberlyst 15 beads / 48 h / Heating
2: thionyl chloride / 2 h / 20 °C
3: 30 percent / AlCl3 / nitrobenzene / 18 h / 20 °C
4: 343 mg / triethylsilane / trifluoroacetic acid / 18 h
With
triethylsilane; aluminium trichloride; thionyl chloride; Amberlyst 15 beads;
In
nitrobenzene; trifluoroacetic acid;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 99 percent / 7percent KOH / H2O; ethanol / other reagents and solvents at various temperatures
2: 65 percent / Amberlyst 15 beads / 48 h / Heating
3: thionyl chloride / 2 h / 20 °C
4: 30 percent / AlCl3 / nitrobenzene / 18 h / 20 °C
5: 343 mg / triethylsilane / trifluoroacetic acid / 18 h
With
triethylsilane; potassium hydroxide; aluminium trichloride; thionyl chloride; Amberlyst 15 beads;
In
ethanol; water; nitrobenzene; trifluoroacetic acid;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: thionyl chloride / 2 h / 20 °C
2: 30 percent / AlCl3 / nitrobenzene / 18 h / 20 °C
3: 343 mg / triethylsilane / trifluoroacetic acid / 18 h
With
triethylsilane; aluminium trichloride; thionyl chloride;
In
nitrobenzene; trifluoroacetic acid;