C₃₅H₃₆O₄S₂

Base Information

• Chemical Name: C₃₅H₃₆O₄S₂
• CAS No.: 1356445-57-2
• Molecular Formula: C₃₅H₃₆O₄S₂
• Molecular Weight: 584.8
• Mol file: 1356445-57-2.mol

Synonyms:

Chemical Property of C₃₅H₃₆O₄S₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₅H₃₆O₄S₂

There total 5 articles about C₃₅H₃₆O₄S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2,6-dimethoxyphenyl)boronic acid (23112-96-1) → C35H36O4S2 (1356445-57-2)

Guidance literature:

Multi-step reaction with 4 steps

1.1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium phosphate / toluene

2.1: boron tribromide / dichloromethane

3.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 0.5 h / 80 °C / Inert atmosphere

3.2: 72 h / 80 °C / Inert atmosphere

4.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / Sonication

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; di-isopropyl azodicarboxylate; boron tribromide; potassium carbonate; triphenylphosphine; potassium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; 1.1: Suzuki-Miyauri coupling / 3.1: Williamson synthesis / 3.2: Williamson synthesis / 4.1: Mitsunobu reaction;

DOI:10.1002/asia.201100524

Reference yield:

C20H14O4S2 (1252579-58-0) → C35H36O4S2 (1356445-57-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 0.5 h / 80 °C / Inert atmosphere

1.2: 72 h / 80 °C / Inert atmosphere

2.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / Sonication

With di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; potassium iodide; In tetrahydrofuran; N,N-dimethyl-formamide; 1.1: Williamson synthesis / 1.2: Williamson synthesis / 2.1: Mitsunobu reaction;

DOI:10.1002/asia.201100524

Reference yield:

3,3'dibromo-2,2'-bithiophene (51751-44-1) → C35H36O4S2 (1356445-57-2)

Guidance literature:

Multi-step reaction with 4 steps

1.1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium phosphate / toluene

2.1: boron tribromide / dichloromethane

3.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 0.5 h / 80 °C / Inert atmosphere

3.2: 72 h / 80 °C / Inert atmosphere

4.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / Sonication

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; di-isopropyl azodicarboxylate; boron tribromide; potassium carbonate; triphenylphosphine; potassium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; 1.1: Suzuki-Miyauri coupling / 3.1: Williamson synthesis / 3.2: Williamson synthesis / 4.1: Mitsunobu reaction;

DOI:10.1002/asia.201100524

upstream raw materials:

C₂₄H₂₂O₄S₂

C₂₀H₁₄O₄S₂

C₃₂H₃₂O₄S₂

allyl alcohol