1,2-di(pentafluorophenyl)ethylene oxide

Base Information

• Chemical Name: 1,2-di(pentafluorophenyl)ethylene oxide
• CAS No.: 960501-43-3
• Molecular Formula: C₁₄H₂F₁₀O
• Molecular Weight: 376.153

Synonyms:

Chemical Property of 1,2-di(pentafluorophenyl)ethylene oxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 1,2-di(pentafluorophenyl)ethylene oxide

There total 3 articles about 1,2-di(pentafluorophenyl)ethylene oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

perfluorobenzaldehyde (653-37-2) → 1,2-di(pentafluorophenyl)ethylene oxide (960501-43-3) + trans-2,3,4,5,6,2′,3′,4′,5′,6′-decafluorostilbene (14992-40-6) + 1,2-bis(pentafluorophenyl)ethanone (24043-89-8)

Guidance literature:

With N,N,N,N,N,N-hexamethylphosphoric triamide; iron pentacarbonyl; In benzene; at 80 ℃; for 4h;

DOI:10.1134/S1070428007040057

Reference yield:

perfluorobenzaldehyde (653-37-2) → 1,2-di(pentafluorophenyl)ethylene oxide (960501-43-3) + trans-2,3,4,5,6,2′,3′,4′,5′,6′-decafluorostilbene (14992-40-6) + 1,2-bis(pentafluorophenyl)ethanone (24043-89-8) + 1,2-bis(pentafluorophenyl)ethene (14992-38-2)

Guidance literature:

With N,N,N,N,N,N-hexamethylphosphoric triamide; iron pentacarbonyl; In benzene; at 80 ℃; for 4h;

DOI:10.1016/j.jfluchem.2008.05.017

Reference yield:

→ 1,2-di(pentafluorophenyl)ethylene oxide (960501-43-3)

Guidance literature:

Pentafluorbenzaldehyd, P(NMe2)3;

DOI:10.1021/jo00937a600

upstream raw materials:

perfluorobenzaldehyde

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