Decane-1,10-diyl dicarbonochloridate

Base Information

• Chemical Name: Decane-1,10-diyl dicarbonochloridate
• CAS No.: 56757-75-6
• Molecular Formula: C12H20 Cl2 O4
• Molecular Weight: 299.194
• NSC Number: 85224
• DSSTox Substance ID: DTXSID40292740
• Nikkaji Number: J1.504.930H
• Wikidata: Q82031168
• Mol file: 56757-75-6.mol

Synonyms:56757-75-6;decane-1,10-diyl dicarbonochloridate;NSC85224;SCHEMBL6036765;DTXSID40292740;NSC-85224

Chemical Property of Decane-1,10-diyl dicarbonochloridate

Chemical Property:

• Vapor Pressure: 3.52E-05mmHg at 25°C
• Boiling Point: 353.7°C at 760 mmHg
• Flash Point: 126.8°C
• Density: 1.167g/cm³
• XLogP3: 5.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 13
• Exact Mass: 298.0738645
• Heavy Atom Count: 18
• Complexity: 210

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(CCCCCOC(=O)Cl)CCCCOC(=O)Cl

Technology Process of Decane-1,10-diyl dicarbonochloridate

There total 2 articles about Decane-1,10-diyl dicarbonochloridate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phosgene (75-44-5) + 1,10-Decanediol (112-47-0) → 1,10-decamethylene glycol dichloroformate (56757-75-6)

Guidance literature:

cooling;

DOI:10.1081/SCC-100000525

Reference yield:

→ 1,10-decamethylene glycol dichloroformate (56757-75-6)

Guidance literature:

Decamethylenglykol, Phosgen, Bzl.;

Reference yield: 97.0%

1,10-decamethylene glycol dichloroformate (56757-75-6) → 1,10-dichlorodecane (2162-98-3)

Guidance literature:

With N,N-dimethyl-formamide; at 130 - 140 ℃;

DOI:10.1021/jo00163a047

upstream raw materials:

phosgene

1,10-Decanediol

Downstream raw materials:

1,10-dichlorodecane