Technology Process of (5S)-3-[(4-methoxyphenyl)methyl]-5-methyl-1,2,3-oxathiazolidine-2,2-dione
There total 4 articles about (5S)-3-[(4-methoxyphenyl)methyl]-5-methyl-1,2,3-oxathiazolidine-2,2-dione which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium periodate; ruthenium(III) chloride trihydrate;
In
water; acetonitrile;
at 0 ℃;
DOI:10.1039/c3ob42512f
- Guidance literature:
-
Multi-step reaction with 4 steps
1: methanol / 50 °C / Molecular sieve
2: sodium tetrahydroborate / 0 - 20 °C
3: thionyl chloride; triethylamine; 1H-imidazole / dichloromethane / 3 h / -60 °C
4: ruthenium(III) chloride trihydrate; sodium periodate / acetonitrile; water / 0 °C
With
1H-imidazole; sodium tetrahydroborate; sodium periodate; thionyl chloride; ruthenium(III) chloride trihydrate; triethylamine;
In
methanol; dichloromethane; water; acetonitrile;
DOI:10.1039/c3ob42512f
- Guidance literature:
-
Multi-step reaction with 2 steps
1: thionyl chloride; triethylamine; 1H-imidazole / dichloromethane / 3 h / -60 °C
2: ruthenium(III) chloride trihydrate; sodium periodate / acetonitrile; water / 0 °C
With
1H-imidazole; sodium periodate; thionyl chloride; ruthenium(III) chloride trihydrate; triethylamine;
In
dichloromethane; water; acetonitrile;
DOI:10.1039/c3ob42512f
