Technology Process of C14H14O3
There total 5 articles about C14H14O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
tert-butyl 3-(2-(3-oxobut-1-ynyl)phenyl)propanoate;
With
trifluoroacetic acid;
methanol;
With
dmap; dicyclohexyl-carbodiimide;
Further stages.;
DOI:10.1055/s-2006-958949
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 93 percent / triethylamine / PdCl2(PPh3)2; CuI
2.1: 94 percent / (COCl)2 / dimethylsulfoxide
3.1: TFA
3.2: 85 percent / DCCl; DMAP
With
oxalyl dichloride; triethylamine; trifluoroacetic acid;
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide;
In
dimethyl sulfoxide;
1.1: Sonogashira coupling reaction / 2.1: Swern oxidation;
DOI:10.1055/s-2006-958949
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 84 percent / formic acid; triethylamine
2.1: 93 percent / triethylamine / PdCl2(PPh3)2; CuI
3.1: 94 percent / (COCl)2 / dimethylsulfoxide
4.1: TFA
4.2: 85 percent / DCCl; DMAP
With
formic acid; oxalyl dichloride; triethylamine; trifluoroacetic acid;
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide;
In
dimethyl sulfoxide;
3.1: Sonogashira coupling reaction / 4.1: Swern oxidation;
DOI:10.1055/s-2006-958949
