thallium methyl 2,3,5,6-tetrafluoro-4-oxybenzoate

Base Information

Chemical Name:thallium methyl 2,3,5,6-tetrafluoro-4-oxybenzoate
CAS No.:1283109-94-3
Molecular Formula:C₈H₃F₄O₃*Tl
Molecular Weight:427.487
Hs Code.:

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Chemical Property of thallium methyl 2,3,5,6-tetrafluoro-4-oxybenzoate

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Technology Process of thallium methyl 2,3,5,6-tetrafluoro-4-oxybenzoate

There total 1 articles about thallium methyl 2,3,5,6-tetrafluoro-4-oxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 58286-07-0
methyl 2,3,5,6-tetrafluoro-4-hydroxybenzoate

: 20398-06-5
thallium (I) ethoxide

: 1283109-94-3
thallium methyl 2,3,5,6-tetrafluoro-4-oxybenzoate

Guidance literature:: In tetrahydrofuran; THF soln. of EtOTl (4.78 mmol) added to THF soln. of MeOC(O)C6F4OH (4.55mmol), suspn. stirred for 3 h; solid collected, washed with THF, dried under vac.; NMR;
DOI:10.1016/j.jorganchem.2011.01.014

Reference yield: 80.0%

: RuCl₂(C,N-(CHCH₂CH₂-2-C₅H₄N))(triisopropylphosphine)

: 1283109-94-3
thallium methyl 2,3,5,6-tetrafluoro-4-oxybenzoate

: Ru(C,N-(CHCH₂CH₂-2-C₅H₄N))(methyl 2,3,5,6-tetrafluoro-4-oxybenzoate)2(triisopropylphosphine)

Guidance literature:: In dichloromethane; dry glovebox techniques used, mixt. of CH2Cl2, Ru(C,N-(CHCH2CH2-2-C5H4N))Cl2(P(iPr)3) (0.44 mmol) and MeOC(O)C6F4OTl (0.90 mmol) stirred overnight at ambient temp.; filtered, filtrate reduced to dryness, recrystd. from CH2Cl2-hexane; XRD;
DOI:10.1016/j.jorganchem.2011.01.014

Reference yield: 77.0%

: 477218-66-9
Grubbs catalyst third generation

: 75-09-2
dichloromethane

: 1283109-94-3
thallium methyl 2,3,5,6-tetrafluoro-4-oxybenzoate

: Ru(benzylidene)(methyl 2,3,5,6-tetrafluoro-4-oxybenzoate)2(bromopyridine)(C₃H₄N₂(mesityl)2)*0.5CH₂Cl₂

Guidance literature:: In dichloromethane; dry glovebox techniques used, mixt. of CH2Cl2, Ru(CHPh)Cl2(BrPy)2(H2IMes) (0.25 mmol) and MeOC(O)C6F4OTl (0.51 mmol) stirred at ambient temp. for 16 h; filtered, filtrate reduced to dryness, washed with CH2Cl2-hexane (1:5, v/v); XRD;
DOI:10.1016/j.jorganchem.2011.01.014