7c-hydroxy-4-hydroxymethyl-2ξ-(4-methoxy-phenyl)-13-methyl-(6ac)-7,11-dihydro-6aH-4r,11ac-azaethano-[1,3,5]dithiazepino[5,4-a]indole-5,12-dione

Base Information

Chemical Name:7c-hydroxy-4-hydroxymethyl-2ξ-(4-methoxy-phenyl)-13-methyl-(6ac)-7,11-dihydro-6aH-4r,11ac-azaethano-[1,3,5]dithiazepino[5,4-a]indole-5,12-dione
CAS No.:61378-02-7
Molecular Formula:C₂₁H₂₂N₂O₅S₂
Molecular Weight:446.548
Hs Code.:

7<i>c</i>-hydroxy-4-hydroxymethyl-2ξ-(4-methoxy-phenyl)-13-methyl-(6a<i>c</i>)-7,11-dihydro-6a<i>H</i>-4<i>r</i>,11a<i>c</i>-azaethano-[1,3,5]dithiazepino[5,4-<i>a</i>]indole-5,12-dione

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Chemical Property of 7c-hydroxy-4-hydroxymethyl-2ξ-(4-methoxy-phenyl)-13-methyl-(6ac)-7,11-dihydro-6aH-4r,11ac-azaethano-[1,3,5]dithiazepino[5,4-a]indole-5,12-dione

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Technology Process of 7c-hydroxy-4-hydroxymethyl-2ξ-(4-methoxy-phenyl)-13-methyl-(6ac)-7,11-dihydro-6aH-4r,11ac-azaethano-[1,3,5]dithiazepino[5,4-a]indole-5,12-dione

There total 52 articles about 7c-hydroxy-4-hydroxymethyl-2ξ-(4-methoxy-phenyl)-13-methyl-(6ac)-7,11-dihydro-6aH-4r,11ac-azaethano-[1,3,5]dithiazepino[5,4-a]indole-5,12-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.8%

: 61378-01-6,79298-64-9,79298-72-9
C₂₈H₂₈N₂O₅S₂

: 61378-02-7,79298-65-0,79298-73-0,79299-13-1
C₂₁H₂₂N₂O₅S₂

Guidance literature:: With boron trichloride; In dichloromethane; at 0 ℃; for 0.166667h;
DOI:10.1016/S0040-4020(01)97960-8

Reference yield: 55.0%

: 61378-01-6,79298-64-9,79298-72-9
C₂₈H₂₈N₂O₅S₂

: 61378-02-7,79298-65-0,79298-73-0,79299-13-1
C₂₁H₂₂N₂O₅S₂

Guidance literature:: With boron trichloride; In dichloromethane; at 0 ℃; for 0.166667h;
DOI:10.1016/S0040-4020(01)97960-8

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 67-99-2
gliotoxin

: 61378-02-7,79298-65-0,79298-73-0,79299-13-1
C₂₁H₂₂N₂O₅S₂

: 61378-02-7,79298-65-0,79298-73-0,79299-13-1
C₂₁H₂₂N₂O₅S₂

Guidance literature:: With sodium tetrahydroborate; boron trifluoride diethyl etherate; Yield given. Multistep reaction. Yields of byproduct given; 1.) CH₂Cl₂, MeOH, 0 deg C; 2.) CH₂Cl₂, MeOH, r.t., 4 h;
DOI:10.1016/S0040-4020(01)97960-8